(E)-ethyl 4-[(4-bromophenyl)(2-(tert-butylamino)-1-(2-nitro-4-(trifluoromethyl)phenyl)-2-oxoethyl)amino]-4-oxobut-2-enoate

Base Information

Chemical Name:(E)-ethyl 4-[(4-bromophenyl)(2-(tert-butylamino)-1-(2-nitro-4-(trifluoromethyl)phenyl)-2-oxoethyl)amino]-4-oxobut-2-enoate
CAS No.:1070901-28-8
Molecular Formula:C₂₅H₂₅BrF₃N₃O₆
Molecular Weight:600.389
Hs Code.:

Synonyms:(E)-ethyl 4-[(4-bromophenyl)(2-(tert-butylamino)-1-(2-nitro-4-(trifluoromethyl)phenyl)-2-oxoethyl)amino]-4-oxobut-2-enoate

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Chemical Property of (E)-ethyl 4-[(4-bromophenyl)(2-(tert-butylamino)-1-(2-nitro-4-(trifluoromethyl)phenyl)-2-oxoethyl)amino]-4-oxobut-2-enoate

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Technology Process of (E)-ethyl 4-[(4-bromophenyl)(2-(tert-butylamino)-1-(2-nitro-4-(trifluoromethyl)phenyl)-2-oxoethyl)amino]-4-oxobut-2-enoate

There total 1 articles about (E)-ethyl 4-[(4-bromophenyl)(2-(tert-butylamino)-1-(2-nitro-4-(trifluoromethyl)phenyl)-2-oxoethyl)amino]-4-oxobut-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2459-05-4
(E)-4-ethoxy-4-oxobut-2-enoic acid

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 109466-87-7
4-(trifluoromethyl)-2-nitrobenzaldehyde

: 106-40-1
4-bromo-aniline

: 1070901-28-8
(E)-ethyl 4-[(4-bromophenyl)(2-(tert-butylamino)-1-(2-nitro-4-(trifluoromethyl)phenyl)-2-oxoethyl)amino]-4-oxobut-2-enoate

Guidance literature:: With lithium chloride; In water;
DOI:10.1021/ol801841m

Reference yield: 75.0%

: 1070901-28-8
(E)-ethyl 4-[(4-bromophenyl)(2-(tert-butylamino)-1-(2-nitro-4-(trifluoromethyl)phenyl)-2-oxoethyl)amino]-4-oxobut-2-enoate

: 1070901-30-2
ethyl (E)-4-((1-(2-amino-4-(trifluoromethyl)phenyl)-2-(tert-butylamino)-2-oxoethyl)(4-bromophenyl)amino)-4-oxobut-2-enoate

: ethyl 2-(4-(4-bromophenyl)-5-(tert-butylcarbamoyl)-3-oxo-8-(trifluoromethyl)-2,3,4,5-tetrahydro-1H-benzo[e][1,4]diazepin-2-yl)acetate

: ethyl 2-(4-(4-bromophenyl)-5-(tert-butylcarbamoyl)-3-oxo-8-(trifluoromethyl)-2,3,4,5-tetrahydro-1H-benzo[e][1,4]diazepin-2-yl)acetate

Guidance literature:: With iron; ammonium chloride; In ethanol; water; at 150 ℃; for 0.75h; under 7500.75 Torr; optical yield given as %de; chemoselective reaction; Microwave irradiation;
DOI:10.1021/ol801841m