diethyl 2,2'-((4-bromo-2-(2-ethoxy-2-oxoethoxy)phenyl)azanediyl)diacetate

Base Information

Chemical Name:diethyl 2,2'-((4-bromo-2-(2-ethoxy-2-oxoethoxy)phenyl)azanediyl)diacetate
CAS No.:864169-19-7
Molecular Formula:C₁₈H₂₄BrNO₇
Molecular Weight:446.295
Hs Code.:

Synonyms:diethyl 2,2'-((4-bromo-2-(2-ethoxy-2-oxoethoxy)phenyl)azanediyl)diacetate

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Chemical Property of diethyl 2,2'-((4-bromo-2-(2-ethoxy-2-oxoethoxy)phenyl)azanediyl)diacetate

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Technology Process of diethyl 2,2'-((4-bromo-2-(2-ethoxy-2-oxoethoxy)phenyl)azanediyl)diacetate

There total 4 articles about diethyl 2,2'-((4-bromo-2-(2-ethoxy-2-oxoethoxy)phenyl)azanediyl)diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 864169-18-6
[(2-ethoxycarbonylmethoxy-phenyl)-ethoxycarbonylmethyl-amino]acetic acid ethyl ester

: 864169-19-7
diethyl 2,2'-((4-bromo-2-(2-ethoxy-2-oxoethoxy)phenyl)azanediyl)diacetate

Guidance literature:: With C₁₂H₂₄O₆*K⁽¹⁺⁾*3Br^(1-); In acetonitrile; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201800013

Reference yield:

: trisodium o-aminophenol-N,N,O-triacetate

: 864169-19-7
diethyl 2,2'-((4-bromo-2-(2-ethoxy-2-oxoethoxy)phenyl)azanediyl)diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 15.8 g / H₂SO₄ / 72 h / Heating

2: 77 percent / Br₂ / CH₂Cl₂ / 2 h / 20 °C

With sulfuric acid; bromine; In dichloromethane; 1: Fischer esterification;
DOI:10.1055/s-2005-869900

Reference yield:

: 95-55-6
2-amino-phenol

: 864169-19-7
diethyl 2,2'-((4-bromo-2-(2-ethoxy-2-oxoethoxy)phenyl)azanediyl)diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaOH / 0.5 h / pH 10.7 / Heating

2: 15.8 g / H₂SO₄ / 72 h / Heating

3: 77 percent / Br₂ / CH₂Cl₂ / 2 h / 20 °C

With sodium hydroxide; sulfuric acid; bromine; In dichloromethane; 2: Fischer esterification;
DOI:10.1055/s-2005-869900