methyl (1S,3R,3aS,6aR)-5-ethyl-4,6-dioxo-3-phenyloctahydro pyrrolo[3,4-c]pyrrole-1-carboxylate

Base Information

Chemical Name:methyl (1S,3R,3aS,6aR)-5-ethyl-4,6-dioxo-3-phenyloctahydro pyrrolo[3,4-c]pyrrole-1-carboxylate
CAS No.:1140972-17-3
Molecular Formula:C₁₆H₁₈N₂O₄
Molecular Weight:302.33
Hs Code.:

Synonyms:methyl (1S,3R,3aS,6aR)-5-ethyl-4,6-dioxo-3-phenyloctahydro pyrrolo[3,4-c]pyrrole-1-carboxylate

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Chemical Property of methyl (1S,3R,3aS,6aR)-5-ethyl-4,6-dioxo-3-phenyloctahydro pyrrolo[3,4-c]pyrrole-1-carboxylate

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Technology Process of methyl (1S,3R,3aS,6aR)-5-ethyl-4,6-dioxo-3-phenyloctahydro pyrrolo[3,4-c]pyrrole-1-carboxylate

There total 2 articles about methyl (1S,3R,3aS,6aR)-5-ethyl-4,6-dioxo-3-phenyloctahydro pyrrolo[3,4-c]pyrrole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 128-53-0
N-Ethylmaleimide

: 66646-88-6
methyl 2-(benzylideneamino)acetate

: 1140972-17-3
methyl (1S,3R,3aS,6aR)-5-ethyl-4,6-dioxo-3-phenyloctahydro pyrrolo[3,4-c]pyrrole-1-carboxylate

Guidance literature:: With (Sa)-Binap-AuTFA; In toluene; at 20 ℃; for 48h; optical yield given as %ee; enantioselective reaction;
DOI:10.1016/j.tetasy.2010.06.011

Reference yield:

: 128-53-0
N-Ethylmaleimide

: 66646-88-6
methyl 2-(benzylideneamino)acetate

: 1140972-17-3
methyl (1S,3R,3aS,6aR)-5-ethyl-4,6-dioxo-3-phenyloctahydro pyrrolo[3,4-c]pyrrole-1-carboxylate

: methyl (1R,3S,3aR,6aS)-5-ethyl-3-phenyl-4,6-dioxooctahydropyrrolo[3,4-c]pyrrole-1-carboxylate

Guidance literature:: With (S)-(+)-(3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-[(1R)-1-phenethyl]amine; silver perchlorate; triethylamine; In toluene; at 0 ℃; for 6h; optical yield given as %ee; enantioselective reaction; Darkness;
DOI:10.1002/ejoc.200900774