4-(4-(2-(diethylamino)acetamido)anilino)-6-(cyclohexylmethoxylformamido)quinazoline

Base Information

Chemical Name:4-(4-(2-(diethylamino)acetamido)anilino)-6-(cyclohexylmethoxylformamido)quinazoline
CAS No.:1451544-43-6
Molecular Formula:C₂₈H₃₆N₆O₃
Molecular Weight:504.632
Hs Code.:

Synonyms:4-(4-(2-(diethylamino)acetamido)anilino)-6-(cyclohexylmethoxylformamido)quinazoline

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Chemical Property of 4-(4-(2-(diethylamino)acetamido)anilino)-6-(cyclohexylmethoxylformamido)quinazoline

Chemical Property:

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Technology Process of 4-(4-(2-(diethylamino)acetamido)anilino)-6-(cyclohexylmethoxylformamido)quinazoline

There total 10 articles about 4-(4-(2-(diethylamino)acetamido)anilino)-6-(cyclohexylmethoxylformamido)quinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.7%

: 1451544-53-8
C₂₀H₂₄N₆O

: 6099-86-1
cyclohexylmethyl chlorocarbonate

: 1451544-43-6
4-(4-(2-(diethylamino)acetamido)anilino)-6-(cyclohexylmethoxylformamido)quinazoline

Guidance literature:: With dmap; In chloroform; at 0 - 20 ℃; for 20h;
DOI:10.1002/cmdc.201300120

Reference yield:

: 1451544-48-1
4-(4-(2-(diethylamino)acetamido)anilino)-6-nitroquinazoline

: 1451544-43-6
4-(4-(2-(diethylamino)acetamido)anilino)-6-(cyclohexylmethoxylformamido)quinazoline

Guidance literature:: Multi-step reaction with 2 steps

1: iron; hydrogenchloride / ethanol; water / 4 h / 20 °C / Reflux

2: dmap / chloroform / 20 h / 0 - 20 °C

With hydrogenchloride; dmap; iron; In ethanol; chloroform; water;
DOI:10.1002/cmdc.201300120

Reference yield:

: 19815-16-8
4-chloro-6-nitro-quinazoline

: 1451544-43-6
4-(4-(2-(diethylamino)acetamido)anilino)-6-(cyclohexylmethoxylformamido)quinazoline

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / isopropyl alcohol / 8 h / Reflux

2: iron; hydrogenchloride / ethanol; water / 4 h / 20 °C / Reflux

3: dmap / chloroform / 20 h / 0 - 20 °C

With hydrogenchloride; dmap; iron; triethylamine; In ethanol; chloroform; water; isopropyl alcohol;
DOI:10.1002/cmdc.201300120