(4S)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-[(3-chlorophenyl)amino]imidazoline

Base Information

Chemical Name:(4S)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-[(3-chlorophenyl)amino]imidazoline
CAS No.:1269603-78-2
Molecular Formula:C₁₉H₂₁ClN₄O₂
Molecular Weight:372.854
Hs Code.:

Synonyms:(4S)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-[(3-chlorophenyl)amino]imidazoline

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Chemical Property of (4S)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-[(3-chlorophenyl)amino]imidazoline

Chemical Property:

Purity/Quality:

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Technology Process of (4S)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-[(3-chlorophenyl)amino]imidazoline

There total 3 articles about (4S)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-[(3-chlorophenyl)amino]imidazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2S)-N⁴-benzyloxycarbonyl-1,2,4-triaminobutane dihydrochloride

: 56721-60-9
1-(3-Chloro-phenyl)-2-methyl-isothiourea; hydriodide

: 1269603-78-2
(4S)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-[(3-chlorophenyl)amino]imidazoline

Guidance literature:: (2S)-N⁴-benzyloxycarbonyl-1,2,4-triaminobutane dihydrochloride; 1-(3-Chloro-phenyl)-2-methyl-isothiourea; hydriodide; In pentan-1-ol; for 24h; Reflux;

With sodium hydroxide; In water; pH=12;
DOI:10.1016/j.bmc.2010.11.039

Reference yield:

: 21258-04-8
N-benzoyl-N′-(3-chlorophenyl)thiourea

: 1269603-78-2
(4S)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-[(3-chlorophenyl)amino]imidazoline

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; sodium hydroxide / 0.67 h / 90 °C

2.1: methanol / 3 h / Reflux

3.1: pentan-1-ol / 24 h / Reflux

3.2: pH 12

With water; sodium hydroxide; In methanol; pentan-1-ol;
DOI:10.1016/j.bmc.2010.11.039

Reference yield:

: 4947-89-1
1-(3-chlorophenyl)-2-thiourea

: 1269603-78-2
(4S)-4-(N-benzyloxycarbonyl-2-aminoethyl)-2-[(3-chlorophenyl)amino]imidazoline

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 3 h / Reflux

2.1: pentan-1-ol / 24 h / Reflux

2.2: pH 12

In methanol; pentan-1-ol;
DOI:10.1016/j.bmc.2010.11.039