(2R,3R)-3-(2',4'-difluorophenyl)-3,4-epoxy-2-(1'-methoxy-1'-methylethoxy)butane

Base Information

Chemical Name:(2R,3R)-3-(2',4'-difluorophenyl)-3,4-epoxy-2-(1'-methoxy-1'-methylethoxy)butane
CAS No.:853243-86-4
Molecular Formula:C₁₄H₁₈F₂O₃
Molecular Weight:272.292
Hs Code.:

Synonyms:(2R,3R)-3-(2',4'-difluorophenyl)-3,4-epoxy-2-(1'-methoxy-1'-methylethoxy)butane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-3-(2',4'-difluorophenyl)-3,4-epoxy-2-(1'-methoxy-1'-methylethoxy)butane

Chemical Property:

Purity/Quality:

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Technology Process of (2R,3R)-3-(2',4'-difluorophenyl)-3,4-epoxy-2-(1'-methoxy-1'-methylethoxy)butane

There total 2 articles about (2R,3R)-3-(2',4'-difluorophenyl)-3,4-epoxy-2-(1'-methoxy-1'-methylethoxy)butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 853243-84-2
(2R)-2',4'-difluoro-2-(1'-methoxy-1'-methylethoxy)propiophenone

: 3084-53-5
trimethylsulphonium bromide

: 853243-86-4
(2R,3R)-3-(2',4'-difluorophenyl)-3,4-epoxy-2-(1'-methoxy-1'-methylethoxy)butane

: C₁₄H₁₈F₂O₃

Guidance literature:: trimethylsulphonium bromide; With sodium hydride; In dimethyl sulfoxide; at 16 - 25 ℃; for 2.5h;

(2R)-2',4'-difluoro-2-(1'-methoxy-1'-methylethoxy)propiophenone; In dimethyl sulfoxide; toluene; paraffin; at 20 ℃; for 3.25h; Product distribution / selectivity;

Reference yield:

: 853243-84-2
(2R)-2',4'-difluoro-2-(1'-methoxy-1'-methylethoxy)propiophenone

: 1774-47-6
trimethylsulfoxonium iodide

: 853243-86-4
(2R,3R)-3-(2',4'-difluorophenyl)-3,4-epoxy-2-(1'-methoxy-1'-methylethoxy)butane

: C₁₄H₁₈F₂O₃

Guidance literature:: (2R)-2',4'-difluoro-2-(1'-methoxy-1'-methylethoxy)propiophenone; trimethylsulfoxonium iodide; With sodium hydride; In tetrahydrofuran; dimethyl sulfoxide; at 10 - 20 ℃;

With sodium hydride; In tetrahydrofuran; dimethyl sulfoxide; at 0 - 5 ℃; Product distribution / selectivity;