(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3-fluoro-4-hydrazinylbenzenesulfonate

Base Information

Chemical Name:(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3-fluoro-4-hydrazinylbenzenesulfonate
CAS No.:1335107-41-9
Molecular Formula:C₁₄H₂₁FN₂O₅S
Molecular Weight:348.396
Hs Code.:

Synonyms:(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3-fluoro-4-hydrazinylbenzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3-fluoro-4-hydrazinylbenzenesulfonate

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Technology Process of (2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3-fluoro-4-hydrazinylbenzenesulfonate

There total 3 articles about (2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3-fluoro-4-hydrazinylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1335107-38-4
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3,4-difluorobenzenesulfonate

: 1335107-41-9
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3-fluoro-4-hydrazinylbenzenesulfonate

Guidance literature:: With hydrazine hydrate; In dimethyl sulfoxide; at 20 ℃;
DOI:10.1021/ja207004v

Reference yield:

: 3663-46-5
5-hydroxymethyl-2,2,5-trimethyl-1,3-dioxane

: 1335107-41-9
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3-fluoro-4-hydrazinylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / acetonitrile / 0 - 20 °C

2: hydrazine hydrate / dimethyl sulfoxide / 20 °C

With pyridine; hydrazine hydrate; In dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ja207004v

Reference yield:

: 145758-05-0
3,4-difluorobenzenesulfonyl chloride

: 1335107-41-9
(2,2,5-trimethyl-1,3-dioxan-5-yl)methyl 3-fluoro-4-hydrazinylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / acetonitrile / 0 - 20 °C

2: hydrazine hydrate / dimethyl sulfoxide / 20 °C

With pyridine; hydrazine hydrate; In dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ja207004v