4-methyl-N-((3-phenyloxiran-2-yl)methyl)-N-(3-phenylprop-2-yn-1-yl)benzenesulfonamide

Base Information

• Chemical Name: 4-methyl-N-((3-phenyloxiran-2-yl)methyl)-N-(3-phenylprop-2-yn-1-yl)benzenesulfonamide
• CAS No.: 1598431-81-2
• Molecular Formula: C₂₅H₂₃NO₃S
• Molecular Weight: 417.529

Synonyms:4-methyl-N-((3-phenyloxiran-2-yl)methyl)-N-(3-phenylprop-2-yn-1-yl)benzenesulfonamide

Chemical Property of 4-methyl-N-((3-phenyloxiran-2-yl)methyl)-N-(3-phenylprop-2-yn-1-yl)benzenesulfonamide

Chemical Property:

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Technology Process of 4-methyl-N-((3-phenyloxiran-2-yl)methyl)-N-(3-phenylprop-2-yn-1-yl)benzenesulfonamide

There total 5 articles about 4-methyl-N-((3-phenyloxiran-2-yl)methyl)-N-(3-phenylprop-2-yn-1-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-N-(3-phenyl-allyl)-N-(3-phenylprop-2-ynyl)benzenesulfonamide (1334688-33-3) → 4-methyl-N-((3-phenyloxiran-2-yl)methyl)-N-(3-phenylprop-2-yn-1-yl)benzenesulfonamide (1598431-81-2)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jo402550e

Reference yield:

toluene-4-sulfonamide (70-55-3) → 4-methyl-N-((3-phenyloxiran-2-yl)methyl)-N-(3-phenylprop-2-yn-1-yl)benzenesulfonamide (1598431-81-2)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 16 h / 60 °C

2: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

With sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; acetone;

DOI:10.1021/jo402550e

Reference yield:

3-bromo-1-phenyl-1-propenyl bromide (4392-24-9) → 4-methyl-N-((3-phenyloxiran-2-yl)methyl)-N-(3-phenylprop-2-yn-1-yl)benzenesulfonamide (1598431-81-2)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 16 h / 60 °C

2: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

With sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; acetone;

DOI:10.1021/jo402550e

upstream raw materials:

3-bromo-1-phenyl-1-propenyl bromide

toluene-4-sulfonamide

4-methyl-N-(3-phenyl-allyl)-N-(3-phenylprop-2-ynyl)benzenesulfonamide

1-bromo-3-phenylprop-2-yne

Downstream raw materials:

phenyl(4-phenyl-1-tosyl-3,4-dehydropiperidin-3-yl)methanone

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