C₃₉H₃₂F₃N₅O₂S

Base Information

Chemical Name:C₃₉H₃₂F₃N₅O₂S
CAS No.:1629023-69-3
Molecular Formula:C₃₉H₃₂F₃N₅O₂S
Molecular Weight:691.777
Hs Code.:

C<sub>39</sub>H<sub>32</sub>F<sub>3</sub>N<sub>5</sub>O<sub>2</sub>S

Synonyms:C₃₉H₃₂F₃N₅O₂S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₉H₃₂F₃N₅O₂S

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Technology Process of C₃₉H₃₂F₃N₅O₂S

There total 15 articles about C₃₉H₃₂F₃N₅O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1629023-86-4
C₃₈H₃₀F₃N₅

: 124-63-0
methanesulfonyl chloride

: 1629023-69-3
C₃₉H₃₂F₃N₅O₂S

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2014.05.082

Reference yield:

: 1620328-45-1
C₃₈H₂₉F₃N₄O

: 1629023-69-3
C₃₉H₃₂F₃N₅O₂S

Guidance literature:: Multi-step reaction with 3 steps

1: diphenyl phosphoryl azide; triphenylphosphine; di-isopropyl azodicarboxylate / 16 h / 0 - 20 °C

2: hydrogen; palladium 10% on activated carbon / methanol; ethyl acetate / 1 h / 20 °C

3: triethylamine / dichloromethane / 2 h / 20 °C

With di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; triethylamine; triphenylphosphine; In methanol; dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2014.05.082

Reference yield:

: 1620328-25-7
C₄₀H₃₁F₃N₄O₂

: 1629023-69-3
C₃₉H₃₂F₃N₅O₂S

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / tetrahydrofuran; methanol / 1 h / 0 °C

2: diphenyl phosphoryl azide; triphenylphosphine; di-isopropyl azodicarboxylate / 16 h / 0 - 20 °C

3: hydrogen; palladium 10% on activated carbon / methanol; ethyl acetate / 1 h / 20 °C

4: triethylamine / dichloromethane / 2 h / 20 °C

With di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2014.05.082