10-[2-(3-Methoxy-phenyl)-ethyl]-3,7,8-trimethyl-10H-benzo[g]pteridine-2,4-dione

Base Information

Chemical Name:10-[2-(3-Methoxy-phenyl)-ethyl]-3,7,8-trimethyl-10H-benzo[g]pteridine-2,4-dione
CAS No.:74235-95-3
Molecular Formula:C₂₂H₂₂N₄O₃
Molecular Weight:390.442
Hs Code.:

Synonyms:10-[2-(3-Methoxy-phenyl)-ethyl]-3,7,8-trimethyl-10H-benzo[g]pteridine-2,4-dione

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Chemical Property of 10-[2-(3-Methoxy-phenyl)-ethyl]-3,7,8-trimethyl-10H-benzo[g]pteridine-2,4-dione

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Technology Process of 10-[2-(3-Methoxy-phenyl)-ethyl]-3,7,8-trimethyl-10H-benzo[g]pteridine-2,4-dione

There total 7 articles about 10-[2-(3-Methoxy-phenyl)-ethyl]-3,7,8-trimethyl-10H-benzo[g]pteridine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 74235-94-2
10-[2-(3-Methoxy-phenyl)-ethyl]-7,8-dimethyl-10H-benzo[g]pteridine-2,4-dione

: 74-88-4
methyl iodide

: 74235-95-3
10-[2-(3-Methoxy-phenyl)-ethyl]-3,7,8-trimethyl-10H-benzo[g]pteridine-2,4-dione

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 23h; Ambient temperature;
DOI:10.1021/ja00535a035

Reference yield:

: 95-64-7
4-amino-o-xylene

: 74235-95-3
10-[2-(3-Methoxy-phenyl)-ethyl]-3,7,8-trimethyl-10H-benzo[g]pteridine-2,4-dione

Guidance literature:: Multi-step reaction with 6 steps

2: 70 percent / LiAlH₄

3: 0.42 g / 0.17 h / 220 °C

4: 0.17 g / NaNO₂ / acetic acid / 1 h / Ambient temperature

5: 69 percent / Na₂S₂O₄ / H₂O; ethanol / 51 h / Ambient temperature

6: 46 percent / K₂CO₃ / dimethylformamide / 23 h / Ambient temperature

With lithium aluminium tetrahydride; sodium dithionite; potassium carbonate; sodium nitrite; In ethanol; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/ja00535a035

Reference yield:

: 74235-90-8
(3,4-Dimethyl-phenyl)-[2-(3-methoxy-phenyl)-ethyl]-amine

: 74235-95-3
10-[2-(3-Methoxy-phenyl)-ethyl]-3,7,8-trimethyl-10H-benzo[g]pteridine-2,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 0.42 g / 0.17 h / 220 °C

2: 0.17 g / NaNO₂ / acetic acid / 1 h / Ambient temperature

3: 69 percent / Na₂S₂O₄ / H₂O; ethanol / 51 h / Ambient temperature

4: 46 percent / K₂CO₃ / dimethylformamide / 23 h / Ambient temperature

With sodium dithionite; potassium carbonate; sodium nitrite; In ethanol; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/ja00535a035