C₃₆H₄₆N₂O₉

Base Information

Chemical Name:C₃₆H₄₆N₂O₉
CAS No.:1438408-23-1
Molecular Formula:C₃₆H₄₆N₂O₉
Molecular Weight:650.769
Hs Code.:

C<sub>36</sub>H<sub>46</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:C₃₆H₄₆N₂O₉

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Chemical Property of C₃₆H₄₆N₂O₉

Chemical Property:

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Technology Process of C₃₆H₄₆N₂O₉

There total 6 articles about C₃₆H₄₆N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1438408-16-2
C₁₄H₂₅NO₄

: 1438408-23-1
C₃₆H₄₆N₂O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / Cooling with ice; Inert atmosphere

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Cooling with ice; Inert atmosphere

2.2: 8 h / 20 °C / Inert atmosphere

2.3: 3.33 h / 20 °C / Inert atmosphere

3.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

5.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

With 1H-imidazole; C₁₅H₂₆Cl₂CuN₂O₂; iodine; caesium carbonate; Dess-Martin periodane; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 4.1: |Dess-Martin Oxidation / 5.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-19-5
C₂₅H₃₈N₂O₇

: 1438408-23-1
C₃₆H₄₆N₂O₉

Guidance literature:: Multi-step reaction with 3 steps

1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

3: dichloromethane / 15 h / 50 °C / Inert atmosphere

With C₁₅H₂₆Cl₂CuN₂O₂; Dess-Martin periodane; triethylamine; In tetrahydrofuran; dichloromethane; 2: |Dess-Martin Oxidation / 3: |Wittig Olefination;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-17-3
C₁₄H₂₄INO₃

: 1438408-23-1
C₃₆H₄₆N₂O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Cooling with ice; Inert atmosphere

1.2: 8 h / 20 °C / Inert atmosphere

1.3: 3.33 h / 20 °C / Inert atmosphere

2.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

4.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

With C₁₅H₂₆Cl₂CuN₂O₂; caesium carbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 3.1: |Dess-Martin Oxidation / 4.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d