N-(2-chlorobenzyl)matrinic acid

Base Information

Chemical Name:N-(2-chlorobenzyl)matrinic acid
CAS No.:1345730-77-9
Molecular Formula:C₂₂H₃₁ClN₂O₂
Molecular Weight:390.953
Hs Code.:

Synonyms:N-(2-chlorobenzyl)matrinic acid

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Chemical Property of N-(2-chlorobenzyl)matrinic acid

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Technology Process of N-(2-chlorobenzyl)matrinic acid

There total 6 articles about N-(2-chlorobenzyl)matrinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₃₆Cl₂N₂O₂

: 1345730-77-9
N-(2-chlorobenzyl)matrinic acid

Guidance literature:: With sodium hydroxide; In ethanol; at 85 ℃; for 4h;
DOI:10.1016/j.bmcl.2021.128503

Reference yield:

: C₃₅H₄₁ClN₂O₂

: 1345730-77-9
N-(2-chlorobenzyl)matrinic acid

Guidance literature:: With 3-methyl-phenol; at 110 ℃;

Reference yield:

: 519-02-8
(+)-matrine

: 1345730-77-9
N-(2-chlorobenzyl)matrinic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / water / 6 h / Reflux

1.2: 3 h / 20 °C

2.1: caesium carbonate / dichloromethane / 20 °C

3.1: sodium hydroxide / methanol / Reflux

With hydrogenchloride; caesium carbonate; sodium hydroxide; In methanol; dichloromethane; water;
DOI:10.1021/acs.jafc.8b04965