1,2-DICHLOROETHYL HYDROPEROXIDE

Base Information

• Chemical Name: 1,2-DICHLOROETHYL HYDROPEROXIDE
• CAS No.: 90584-32-0
• Molecular Formula: C₂H₄Cl₂O₂
• Molecular Weight: 130.959
• Mol file: 90584-32-0.mol

Synonyms:

Chemical Property of 1,2-DICHLOROETHYL HYDROPEROXIDE

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s): 3
• Hazard Codes: 3

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2-DICHLOROETHYL HYDROPEROXIDE

There total 2 articles about 1,2-DICHLOROETHYL HYDROPEROXIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-2,3-dichloro-2-butene (1587-29-7) → 1,1-Dichloroethyl hydroperoxide (90584-32-0) + acetyl chloride (75-36-5)

Guidance literature:

With hydrogenchloride; ozone; In various solvent(s); at 0 ℃; Mechanism;

DOI:10.1021/jo00189a012

Reference yield:

2,3-dichloro-2-butene (4279-21-4) → 1,1-Dichloroethyl hydroperoxide (90584-32-0) + acetyl chloride (75-36-5)

Guidance literature:

With hydrogenchloride; ozone; formic acid ethyl ester; at -10 - 0 ℃;

Reference yield:

1,1-Dichloroethyl hydroperoxide (90584-32-0) → peracetic acid (79-21-0)

Guidance literature:

With water; In chloroform-d1; at 0 ℃; for 0.166667h; Mechanism; Dioxane-d8, -10 deg C;

DOI:10.1021/jo00189a012

upstream raw materials:

(E)-2,3-dichloro-2-butene

2,3-dichloro-2-butene

Downstream raw materials:

peracetic acid

Peressigsaeure-1,1-dichlorethylester

Refernces

• 1、 Gaeb, Siegmar,Turner, Walter V.. "1,1-Dichloroethyl Hydroperoxide and 1,1-Dichloroethyl Peroxide Ion as Intermediates in the Ozonolysis of 2,3-Dichloro-2-butene". . p. 2711 - 2714. Retrieved 2007/10/02.