phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2-deoxy-4-O-methyl-α-D-mannopyranoside

Base Information

Chemical Name:phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2-deoxy-4-O-methyl-α-D-mannopyranoside
CAS No.:161614-94-4
Molecular Formula:C₃₀H₃₁NO₈
Molecular Weight:533.578
Hs Code.:

Synonyms:phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2-deoxy-4-O-methyl-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2-deoxy-4-O-methyl-α-D-mannopyranoside

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Technology Process of phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2-deoxy-4-O-methyl-α-D-mannopyranoside

There total 4 articles about phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2-deoxy-4-O-methyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 161614-91-1
phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2-deoxy-α-D-mannopyranoside

: 74-88-4
methyl iodide

: 161614-94-4
phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2-deoxy-4-O-methyl-α-D-mannopyranoside

Guidance literature:: With silver(l) oxide; In N,N-dimethyl-formamide; for 24h;
DOI:10.1016/S0957-4166(00)80390-0

Reference yield:

: 10375-65-2
phenylmethyl 3,4,6-tri-O-acetyl-2-acetylamino-2-deoxy-α-D-mannopyranoside

: 161614-94-4
phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2-deoxy-4-O-methyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / NaOMe / methanol / 5 h

2: 47 percent / pyridine / CH₂Cl₂ / 24 h

3: 46 percent / Ag₂O / dimethylformamide / 24 h

With pyridine; sodium methylate; silver(l) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0957-4166(00)80390-0

Reference yield:

: 3006-60-8,4539-83-7,6730-10-5,7772-79-4,7784-54-5,10385-50-9,14086-90-9,26151-16-6,76375-60-5,95341-98-3,95341-99-4,134451-91-5,134451-96-0,136982-81-5,145375-11-7,148347-15-3,76375-61-6
1,3,4,6-tetra-O-acetyl-2-acetamido-2-deoxy-α,β-D-mannopyranose

: 161614-94-4
phenylmethyl 2-acetylamino-3,6-di-O-benzoyl-2-deoxy-4-O-methyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 63 percent / BF₃*Et₂O / nitromethane / 1 h / 80 °C

2: 100 percent / NaOMe / methanol / 5 h

3: 47 percent / pyridine / CH₂Cl₂ / 24 h

4: 46 percent / Ag₂O / dimethylformamide / 24 h

With pyridine; boron trifluoride diethyl etherate; sodium methylate; silver(l) oxide; In methanol; nitromethane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0957-4166(00)80390-0