Technology Process of C26H38N2O7
There total 10 articles about C26H38N2O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 86 percent / HCl
2: HCO2H / Pd/C / methanol / 30 °C
3: 98 percent / TiCl4 / CH2Cl2 / 0 °C
4: Et3N; DMAP
5: K2CO3 / H2O
6: Ag2O / dimethylformamide
7: LiOH; H2O / tetrahydrofuran; methanol
8: HATU; DIPEA
With
hydrogenchloride; dmap; lithium hydroxide; formic acid; water; titanium tetrachloride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; silver(l) oxide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.07.142
- Guidance literature:
-
Multi-step reaction with 8 steps
1: HCO2H / Pd/C / methanol / 30 °C
2: 98 percent / TiCl4 / CH2Cl2 / 0 °C
3: Et3N; DMAP
4: K2CO3 / H2O
5: Ag2O / dimethylformamide
6: LiOH; H2O / tetrahydrofuran; methanol
7: HATU; DIPEA
With
dmap; lithium hydroxide; formic acid; water; titanium tetrachloride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; silver(l) oxide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.07.142
- Guidance literature:
-
Multi-step reaction with 10 steps
1.1: methanol / 20 °C
1.2: 78 percent / methanol / 80 °C
2.1: 86 percent / HCl
3.1: HCO2H / Pd/C / methanol / 30 °C
4.1: 98 percent / TiCl4 / CH2Cl2 / 0 °C
5.1: Et3N; DMAP
6.1: K2CO3 / H2O
7.1: Ag2O / dimethylformamide
8.1: LiOH; H2O / tetrahydrofuran; methanol
9.1: HATU; DIPEA
With
hydrogenchloride; dmap; lithium hydroxide; formic acid; water; titanium tetrachloride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; silver(l) oxide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
1.1: Strecker reaction;
DOI:10.1016/j.tetlet.2007.07.142