(S)-methyl 2-[(tert-butoxycarbonyl)(methyl)amino]-3-(5-formyl-2-methoxyphenyl)propionate

Base Information

Chemical Name:(S)-methyl 2-[(tert-butoxycarbonyl)(methyl)amino]-3-(5-formyl-2-methoxyphenyl)propionate
CAS No.:944412-25-3
Molecular Formula:C₁₈H₂₅NO₆
Molecular Weight:351.4
Hs Code.:

Synonyms:(S)-methyl 2-[(tert-butoxycarbonyl)(methyl)amino]-3-(5-formyl-2-methoxyphenyl)propionate

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Chemical Property of (S)-methyl 2-[(tert-butoxycarbonyl)(methyl)amino]-3-(5-formyl-2-methoxyphenyl)propionate

Chemical Property:

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Technology Process of (S)-methyl 2-[(tert-butoxycarbonyl)(methyl)amino]-3-(5-formyl-2-methoxyphenyl)propionate

There total 9 articles about (S)-methyl 2-[(tert-butoxycarbonyl)(methyl)amino]-3-(5-formyl-2-methoxyphenyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: (S)-methyl 2-[(tert-butoxycarbonyl)(methyl)amino]-3-(5-(hydroxymethyl)-2-methoxyphenyl)propionate

: 944412-25-3
(S)-methyl 2-[(tert-butoxycarbonyl)(methyl)amino]-3-(5-formyl-2-methoxyphenyl)propionate

Guidance literature:: With 2,6-dimethylpyridine; Dess-Martin periodane; In dichloromethane; at 0 ℃; for 0.666667h;
DOI:10.1021/jo070517u

Reference yield:

: 953809-80-8
C₁₉H₂₃NO₄

: 944412-25-3
(S)-methyl 2-[(tert-butoxycarbonyl)(methyl)amino]-3-(5-formyl-2-methoxyphenyl)propionate

Guidance literature:: Multi-step reaction with 6 steps

1: HCO₂H / Pd/C / methanol / 30 °C

2: 98 percent / TiCl₄ / CH₂Cl₂ / 0 °C

3: Et₃N; DMAP

4: K₂CO₃ / H₂O

5: Ag₂O / dimethylformamide

With dmap; formic acid; titanium tetrachloride; potassium carbonate; triethylamine; silver(l) oxide; palladium on activated charcoal; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.07.142

Reference yield:

: 953809-79-5
C₁₈H₂₀N₂O₂

: 944412-25-3
(S)-methyl 2-[(tert-butoxycarbonyl)(methyl)amino]-3-(5-formyl-2-methoxyphenyl)propionate

Guidance literature:: Multi-step reaction with 7 steps

1: 86 percent / HCl

2: HCO₂H / Pd/C / methanol / 30 °C

3: 98 percent / TiCl₄ / CH₂Cl₂ / 0 °C

4: Et₃N; DMAP

5: K₂CO₃ / H₂O

6: Ag₂O / dimethylformamide

With hydrogenchloride; dmap; formic acid; titanium tetrachloride; potassium carbonate; triethylamine; silver(l) oxide; palladium on activated charcoal; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.07.142