tert-butyl cis-4-hydroxy-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)cyclohexanecarboxylate

Base Information

• Chemical Name: tert-butyl cis-4-hydroxy-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)cyclohexanecarboxylate
• CAS No.: 1010086-49-3
• Molecular Formula: C₂₂H₃₁N₃O₄S
• Molecular Weight: 433.572

Synonyms:tert-butyl cis-4-hydroxy-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)cyclohexanecarboxylate

Chemical Property of tert-butyl cis-4-hydroxy-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)cyclohexanecarboxylate

Chemical Property:

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Technology Process of tert-butyl cis-4-hydroxy-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)cyclohexanecarboxylate

There total 1 articles about tert-butyl cis-4-hydroxy-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl cis-4-((tert-butyl(diphenyl)silyl)oxy)-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)cyclohexanecarboxylate (1010086-47-1) → tert-butyl cis-4-hydroxy-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)cyclohexanecarboxylate (1010086-49-3)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 - 60 ℃;

Reference yield:

tert-butyl cis-4-hydroxy-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)cyclohexanecarboxylate (1010086-49-3) + 2-fluoro-3-chlorophenol (2613-22-1) → tert-butyl trans-4-(3-chloro-2-fluorophenoxy)-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)cyclohexanecarboxylate (1010086-51-7)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

Reference yield:

tert-butyl cis-4-hydroxy-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)cyclohexanecarboxylate (1010086-49-3) + methanesulfonyl chloride (124-63-0) → tert-butyl cis-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)-4-((methylsulfonyl)oxy)cyclohexanecarboxylate

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h;

upstream raw materials:

tert-butyl cis-4-((tert-butyl(diphenyl)silyl)oxy)-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)cyclohexanecarboxylate

Downstream raw materials:

tert-butyl trans-4-(3-chloro-2-fluorophenoxy)-1-((6-(((2Z)-3-(methoxymethyl)-1,3-thiazol-2(3H)-ylidene)amino)pyridin-2-yl)methyl)cyclohexanecarboxylate

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