Acetic acidto,2-diazo-, (2E)-2-buten-1-yl ester

Base Information Edit

Chemical Name:Acetic acidto,2-diazo-, (2E)-2-buten-1-yl ester
CAS No.:14746-03-3
Molecular Formula:C6H8 N2 O2
Molecular Weight:140.142
Hs Code.:
Mol file:14746-03-3.mol

Synonyms:Aceticacid, diazo-, (2E)-2-butenyl ester (9CI); Acetic acid, diazo-, 2-butenyl ester,(E)- (8CI); 2-Buten-1-ol, diazoacetate, (E)- (8CI); trans-2-Butenyldiazoacetate

Suppliers and Price of Acetic acidto,2-diazo-, (2E)-2-buten-1-yl ester

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Acetic acidto,2-diazo-, (2E)-2-buten-1-yl ester Edit

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s): 3
Hazard Codes: 3:;
Safety Statements:Potentially explosive. When heated to decomposition it emits toxic fumes of "> x. See also other diazo compounds." target="_blank">Potentially explosive. When heated to decomposition it emits toxic fumes of

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Acetic acidto,2-diazo-, (2E)-2-buten-1-yl ester

There total 2 articles about Acetic acidto,2-diazo-, (2E)-2-buten-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2158-14-7
4-acetamidobenzenesulfonyl azide

: 82259-92-5
(E)-but-2-en-1-yl 3-oxobutanoate

: 14746-03-3
trans-2-buten-1-yl diazoacetate

Guidance literature:: With lithium hydroxide; triethylamine; In water; acetonitrile;

Reference yield: 72.0%

: 504-61-0,542-72-3
(E)-but-2-enol

: 2158-14-7
4-acetamidobenzenesulfonyl azide

: 5394-63-8
2,2,6-trimethyl-4H-1,3-dioxin-4-one

: 14746-03-3
trans-2-buten-1-yl diazoacetate

Guidance literature:: (E)-but-2-enol; 2,2,6-trimethyl-4H-1,3-dioxin-4-one; In tetrahydrofuran; Heating;

4-acetamidobenzenesulfonyl azide; In acetonitrile; at 20 ℃;

With lithium hydroxide;
DOI:10.1016/S0960-894X(02)00793-X

Reference yield: 52.0%

: 1746-23-2,26009-55-2
4-tert-Butylstyrene

: 14746-03-3
trans-2-buten-1-yl diazoacetate

: (E)-but-2-en-1-yl 5-(4-(tert-butyl)phenyl)-4,5-dihydroisoxazole-3-carboxylate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; tert.-butylnitrite; copper(II) acetate monohydrate; In toluene; at 80 ℃; for 12h; Sealed tube;
DOI:10.1021/acs.orglett.7b02885