2-(4-(trifluoromethyl)phenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

Base Information

Chemical Name:2-(4-(trifluoromethyl)phenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine
CAS No.:1159803-59-4
Molecular Formula:C₁₇H₁₂BF₃N₂
Molecular Weight:312.102
Hs Code.:

Synonyms:2-(4-(trifluoromethyl)phenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

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Chemical Property of 2-(4-(trifluoromethyl)phenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

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Technology Process of 2-(4-(trifluoromethyl)phenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

There total 9 articles about 2-(4-(trifluoromethyl)phenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 128796-39-4
4-trifluoromethylphenylboronic acid

: 479-27-6
naphthalene-1,8-diamine

: 1159803-59-4
2-(4-(trifluoromethyl)phenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

Guidance literature:: In water; at 60 ℃; for 2h; Green chemistry;
DOI:10.1016/j.tet.2021.132205

Reference yield: 94.0%

: 1214264-88-6
2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

: 402-43-7
p-trifluoromethylphenyl bromide

: 1159803-59-4
2-(4-(trifluoromethyl)phenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium acetate; XPhos; In 1,4-dioxane; at 60 ℃; for 12h; chemoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1039/c5cc00231a

Reference yield: 90.0%

: 402-43-7
p-trifluoromethylphenyl bromide

: 5656-71-3
2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

: 1159803-59-4
2-(4-(trifluoromethyl)phenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

Guidance literature:: p-trifluoromethylphenyl bromide; With iodine; magnesium; In tetrahydrofuran; at 20 ℃; for 1h; Schlenk technique; Inert atmosphere;

2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine; In tetrahydrofuran; at 20 ℃; for 3h; Schlenk technique; Inert atmosphere;
DOI:10.1039/d0cc02560g