N-(2-Chloro-5-methylphenyl)hydroxylamine

Base Information

Chemical Name:N-(2-Chloro-5-methylphenyl)hydroxylamine
CAS No.:65039-20-5
Molecular Formula:C₇H₈ClNO
Molecular Weight:157.6
Hs Code.:
DSSTox Substance ID:DTXSID101283717
Nikkaji Number:J1.449.152J

Synonyms:65039-20-5;N-(2-Chloro-5-methylphenyl)hydroxylamine;SCHEMBL11404618;DTXSID101283717;2-Chloro-N-hydroxy-5-methylbenzenamine

Suppliers and Price of N-(2-Chloro-5-methylphenyl)hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N-(2-Chloro-5-methylphenyl)hydroxylamine

Chemical Property:

Refractive Index:1.5430 (estimate)
Boiling Point:140°C (rough estimate)
PSA：32.26000
Density:1.1760 (rough estimate)
LogP:2.52250
XLogP3:2.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:157.0294416
Heavy Atom Count:10
Complexity:110

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s): 3
Hazard Codes:3

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)Cl)NO

Technology Process of N-(2-Chloro-5-methylphenyl)hydroxylamine

There total 2 articles about N-(2-Chloro-5-methylphenyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 89-60-1
1-chloro-4-methyl-2-nitro-benzene

: 65039-20-5
N-(2-Chloro-5-methylphenyl)-hydroxylamine

Guidance literature:: With hydrazine hydrate; Raney nickel (type W-4); In ethanol; 1,2-dichloro-ethane; at 10 ℃; for 4h;
DOI:10.1055/s-1984-31027

Reference yield:

: 65039-20-5
N-(2-Chloro-5-methylphenyl)-hydroxylamine

Guidance literature:: Verb. /BRN= 511055/, Hydrazin;
DOI:10.1055/s-1977-24602

Reference yield: 59.0%

: 65039-20-5
N-(2-Chloro-5-methylphenyl)-hydroxylamine

: 98-88-4
benzoyl chloride

: 96127-02-5
N-(2-chloro-5-methylphenyl)-N-hydroxybenzamide

Guidance literature:: With sodium hydrogencarbonate; In diethyl ether; water; at 0 ℃; for 0.00277778h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.1c03779