1-(L-tyrosyl)aminocyclopropane-1-carbonylglycyl-L-phenylalanyl-L-leucine

Base Information

Chemical Name:1-(L-tyrosyl)aminocyclopropane-1-carbonylglycyl-L-phenylalanyl-L-leucine
CAS No.:80971-87-5
Molecular Formula:C₃₀H₃₉N₅O₇
Molecular Weight:581.669
Hs Code.:

Synonyms:1-(L-tyrosyl)aminocyclopropane-1-carbonylglycyl-L-phenylalanyl-L-leucine

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Chemical Property of 1-(L-tyrosyl)aminocyclopropane-1-carbonylglycyl-L-phenylalanyl-L-leucine

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Technology Process of 1-(L-tyrosyl)aminocyclopropane-1-carbonylglycyl-L-phenylalanyl-L-leucine

There total 8 articles about 1-(L-tyrosyl)aminocyclopropane-1-carbonylglycyl-L-phenylalanyl-L-leucine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 80971-85-3
(S)-2-{(S)-2-[2-({1-[(S)-3-(4-Acetoxy-phenyl)-2-amino-propionylamino]-cyclopropanecarbonyl}-amino)-acetylamino]-3-phenyl-propionylamino}-4-methyl-pentanoic acid

: 80971-87-5
1-(L-tyrosyl)aminocyclopropane-1-carbonylglycyl-L-phenylalanyl-L-leucine

Guidance literature:: With ammonia; In methanol;

Reference yield:

: 3978-80-1
Boc-Tyr-OH

: 80971-87-5
1-(L-tyrosyl)aminocyclopropane-1-carbonylglycyl-L-phenylalanyl-L-leucine

Guidance literature:: Multi-step reaction with 5 steps

1: 2 M NaOH / 0 °C

2: 98 percent / Et₃N, N,N'-dicyclohexylcarbodiimide / dimethylformamide

3: 4 M HCl / dioxane / 1.5 h / Ambient temperature

4: 1.) CF₃COOH, anisole, 2.) IR-45(OAc)

5: 88 percent / NH₃ / methanol

With hydrogenchloride; sodium hydroxide; IR-45(OAc); ammonia; methoxybenzene; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;

Reference yield:

: 80971-82-0
(S)-3-(4-acetoxyphenyl)-2-[N-(tert.butoxycarbonyl)amino]propionic acid

: 80971-87-5
1-(L-tyrosyl)aminocyclopropane-1-carbonylglycyl-L-phenylalanyl-L-leucine

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / Et₃N, N,N'-dicyclohexylcarbodiimide / dimethylformamide

2: 4 M HCl / dioxane / 1.5 h / Ambient temperature

3: 1.) CF₃COOH, anisole, 2.) IR-45(OAc)

4: 88 percent / NH₃ / methanol

With hydrogenchloride; IR-45(OAc); ammonia; methoxybenzene; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;