4-(2-aminoacetylamino)-3-methoxybenzoic acid methyl ester hydrochloride

Base Information

Chemical Name:4-(2-aminoacetylamino)-3-methoxybenzoic acid methyl ester hydrochloride
CAS No.:1419186-19-8
Molecular Formula:C₁₁H₁₄N₂O₄*ClH
Molecular Weight:274.704
Hs Code.:

Synonyms:4-(2-aminoacetylamino)-3-methoxybenzoic acid methyl ester hydrochloride

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Chemical Property of 4-(2-aminoacetylamino)-3-methoxybenzoic acid methyl ester hydrochloride

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Technology Process of 4-(2-aminoacetylamino)-3-methoxybenzoic acid methyl ester hydrochloride

There total 4 articles about 4-(2-aminoacetylamino)-3-methoxybenzoic acid methyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.7%

: Boc-glycine

: 41608-64-4
methyl 3-methoxy-4-aminobenzoate

: 1419186-19-8
4-(2-aminoacetylamino)-3-methoxybenzoic acid methyl ester hydrochloride

Guidance literature:: Boc-glycine; methyl 3-methoxy-4-aminobenzoate; With 4-methyl-morpholine; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; In ethyl acetate; at 0 - 20 ℃;

With hydrogenchloride; In water; ethyl acetate;
DOI:10.1021/op3003213

Reference yield: 69.0%

: 4-(2-((tert-butoxycarbonyl)amino)acetamido)-3-methoxybenzoic acid methyl ester

: 1419186-19-8
4-(2-aminoacetylamino)-3-methoxybenzoic acid methyl ester hydrochloride

Guidance literature:: With hydrogenchloride; In water; ethyl acetate; at 20 ℃;

Reference yield:

: 41608-64-4
methyl 3-methoxy-4-aminobenzoate

: 1419186-19-8
4-(2-aminoacetylamino)-3-methoxybenzoic acid methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; acetyl chloride / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: hydrogenchloride / ethyl acetate; water / 20 °C

With hydrogenchloride; triethylamine; acetyl chloride; In dichloromethane; water; ethyl acetate;