1-{3-chloro-2-[(diphenylphosphanyl)oxy]propyl}-3-methylimidazolium chloride

Base Information

• Chemical Name: 1-{3-chloro-2-[(diphenylphosphanyl)oxy]propyl}-3-methylimidazolium chloride
• CAS No.: 1621393-72-3
• Molecular Formula: C₁₉H₂₁ClN₂OP*Cl
• Molecular Weight: 395.268

Synonyms:1-{3-chloro-2-[(diphenylphosphanyl)oxy]propyl}-3-methylimidazolium chloride

Chemical Property of 1-{3-chloro-2-[(diphenylphosphanyl)oxy]propyl}-3-methylimidazolium chloride

Chemical Property:

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Technology Process of 1-{3-chloro-2-[(diphenylphosphanyl)oxy]propyl}-3-methylimidazolium chloride

There total 1 articles about 1-{3-chloro-2-[(diphenylphosphanyl)oxy]propyl}-3-methylimidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.8%

1-chloro-3-(3-methylimidazolidin-1-yl)propan-2-ol chloride (1118072-24-4) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → 1-{3-chloro-2-[(diphenylphosphanyl)oxy]propyl}-3-methylimidazolium chloride (1621393-72-3)

Guidance literature:

1-chloro-3-(3-methylimidazolidin-1-yl)propan-2-ol chloride; With n-butyllithium; In hexane; dichloromethane; at -78 - 20 ℃; for 1.5h; Inert atmosphere; Schlenk technique;

chloro-diphenylphosphine; In hexane; dichloromethane; at -78 - 20 ℃; for 2h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.poly.2014.05.079

Reference yield: 92.1%

dichloro(benzene)ruthenium(II) dimer (37366-09-9) + 1-{3-chloro-2-[(diphenylphosphanyl)oxy]propyl}-3-methylimidazolium chloride (1621393-72-3) → [Ru((Ph2PO)-C7H14N2Cl)(η6-benzene)Cl2]Cl (1621393-74-5)

Guidance literature:

In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.poly.2014.05.079

Reference yield: 91.6%

[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 (52462-29-0) + 1-{3-chloro-2-[(diphenylphosphanyl)oxy]propyl}-3-methylimidazolium chloride (1621393-72-3) → [Ru((Ph2PO)-C7H14N2Cl)(η6-p-cymene)Cl2]Cl (1621393-77-8)

Guidance literature:

In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.poly.2014.05.079

upstream raw materials:

1-chloro-3-(3-methylimidazolidin-1-yl)propan-2-ol chloride

chloro-diphenylphosphine

Downstream raw materials:

[Ru((Ph₂PO)-C₇H₁₄N₂Cl)(η⁶-benzene)Cl₂]Cl

[Ru((Ph₂PO)-C₇H₁₄N₂Cl)(η⁶-p-cymene)Cl₂]Cl

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