Technology Process of C17H16N2O4S2
There total 6 articles about C17H16N2O4S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H14N2S2; methyl iodide;
In
methanol;
Reflux;
With
potassium peroxymonosulfate;
In
tetrahydrofuran; methanol; water;
at 0 ℃;
for 18h;
DOI:10.1016/j.bmc.2013.01.058
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: phosphoric acid; trifluoroacetic anhydride / 25 °C
2.1: bromine; acetic acid / 20 °C
3.1: sodium methylate / methanol / Reflux
4.1: butan-1-ol / Reflux
5.1: methanol / Reflux
5.2: 18 h / 0 °C
With
phosphoric acid; bromine; sodium methylate; acetic acid; trifluoroacetic anhydride;
In
methanol; butan-1-ol;
DOI:10.1016/j.bmc.2013.01.058
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: bromine; acetic acid / 20 °C
2.1: sodium methylate / methanol / Reflux
3.1: butan-1-ol / Reflux
4.1: methanol / Reflux
4.2: 18 h / 0 °C
With
bromine; sodium methylate; acetic acid;
In
methanol; butan-1-ol;
DOI:10.1016/j.bmc.2013.01.058