(2S,3S)-N²-benzyl-3-(tert-butoxycarbonylamino)-2-(hydroxyamino)-4-methylpentane

Base Information

Chemical Name:(2S,3S)-N²-benzyl-3-(tert-butoxycarbonylamino)-2-(hydroxyamino)-4-methylpentane
CAS No.:195059-46-2
Molecular Formula:C₁₈H₃₀N₂O₃
Molecular Weight:322.448
Hs Code.:

(2S,3S)-N<sup>2</sup>-benzyl-3-(tert-butoxycarbonylamino)-2-(hydroxyamino)-4-methylpentane

Synonyms:(2S,3S)-N²-benzyl-3-(tert-butoxycarbonylamino)-2-(hydroxyamino)-4-methylpentane

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Chemical Property of (2S,3S)-N²-benzyl-3-(tert-butoxycarbonylamino)-2-(hydroxyamino)-4-methylpentane

Chemical Property:

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Technology Process of (2S,3S)-N²-benzyl-3-(tert-butoxycarbonylamino)-2-(hydroxyamino)-4-methylpentane

There total 3 articles about (2S,3S)-N²-benzyl-3-(tert-butoxycarbonylamino)-2-(hydroxyamino)-4-methylpentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 75-16-1
methylmagnesium bromide

: 195059-41-7
(Z)-N-[(2S)-2-(tert-butoxycarbonylamino)-1-methylbutylidene] benzylamine N-oxide

: 195059-46-2
(2S,3S)-N²-benzyl-3-(tert-butoxycarbonylamino)-2-(hydroxyamino)-4-methylpentane

: 195059-47-3
(2R,3S)-N²-benzyl-3-(tert-butoxycarbonylamino)-2-(hydroxyamino)-4-methylpentane

Guidance literature:: In tetrahydrofuran; at -40 ℃; for 4h;
DOI:10.1016/S0957-4166(97)00250-4

Reference yield:

: 79069-51-5
(S)-N-tert-butoxycarbonylvalinal

: 195059-46-2
(2S,3S)-N²-benzyl-3-(tert-butoxycarbonylamino)-2-(hydroxyamino)-4-methylpentane

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / MgSO₄ / CH₂Cl₂ / 4 h / 20 °C

2: 49 percent / tetrahydrofuran / 4 h / -40 °C

With magnesium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0957-4166(97)00250-4

Reference yield:

: 622-30-0
N-benzyl hydroxylalmine

: 195059-46-2
(2S,3S)-N²-benzyl-3-(tert-butoxycarbonylamino)-2-(hydroxyamino)-4-methylpentane

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / MgSO₄ / CH₂Cl₂ / 4 h / 20 °C

2: 49 percent / tetrahydrofuran / 4 h / -40 °C

With magnesium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0957-4166(97)00250-4