5-(4-fluorophenoxy)-2-isopropoxynicotinic acid

Base Information

Chemical Name:5-(4-fluorophenoxy)-2-isopropoxynicotinic acid
CAS No.:1336911-02-4
Molecular Formula:C₁₅H₁₄FNO₄
Molecular Weight:291.279
Hs Code.:

Synonyms:5-(4-fluorophenoxy)-2-isopropoxynicotinic acid

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Chemical Property of 5-(4-fluorophenoxy)-2-isopropoxynicotinic acid

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Technology Process of 5-(4-fluorophenoxy)-2-isopropoxynicotinic acid

There total 6 articles about 5-(4-fluorophenoxy)-2-isopropoxynicotinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1336911-01-3
5-(4-fluorophenoxy)-2-isopropoxypyridine-3-carbaldehyde

: 1336911-02-4
5-(4-fluorophenoxy)-2-isopropoxynicotinic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; In water; tert-butyl alcohol; for 16h;

Reference yield:

: 371-41-5
4-Fluorophenol

: 1336911-02-4
5-(4-fluorophenoxy)-2-isopropoxynicotinic acid

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydride / dimethyl sulfoxide; mineral oil / 16 h / 120 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / 5 h / 20 °C / Reflux

3: trichlorophosphate / 3 h / 120 °C

4: sodium hydride / tetrahydrofuran; mineral oil / 16 h / 50 °C

5: diisobutylaluminium hydride / toluene / 16 h / 0 - 20 °C

6: sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 16 h

With sodium chlorite; sodium dihydrogenphosphate; sodium hydride; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In tetrahydrofuran; water; dimethyl sulfoxide; toluene; mineral oil; tert-butyl alcohol;

Reference yield:

: 35590-37-5
5-bromopyridine-3-carbonitrile

: 1336911-02-4
5-(4-fluorophenoxy)-2-isopropoxynicotinic acid

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydride / dimethyl sulfoxide; mineral oil / 16 h / 120 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / 5 h / 20 °C / Reflux

3: trichlorophosphate / 3 h / 120 °C

4: sodium hydride / tetrahydrofuran; mineral oil / 16 h / 50 °C

5: diisobutylaluminium hydride / toluene / 16 h / 0 - 20 °C

6: sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 16 h

With sodium chlorite; sodium dihydrogenphosphate; sodium hydride; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In tetrahydrofuran; water; dimethyl sulfoxide; toluene; mineral oil; tert-butyl alcohol;