C₂₈H₅₂N₂O₈Si₂

Base Information

• Chemical Name: C₂₈H₅₂N₂O₈Si₂
• CAS No.: 1409937-10-5
• Molecular Formula: C₂₈H₅₂N₂O₈Si₂
• Molecular Weight: 600.9
• Mol file: 1409937-10-5.mol

Synonyms:C₂₈H₅₂N₂O₈Si₂

Chemical Property of C₂₈H₅₂N₂O₈Si₂

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₂₈H₅₂N₂O₈Si₂

There total 2 articles about C₂₈H₅₂N₂O₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

3,6-dimethyl-4,5-dinitrobenzene-1,2-diol (1409937-09-2) + (R)-3-(tert-butyldimethylsilyloxy)-2-methylpropan-1-ol (112057-64-4) → C28H52N2O8Si2 (1409937-10-5)

Guidance literature:

With cyanomethylenetributyl-phosphorane; In tetrahydrofuran; at 80 ℃; for 24h; Inert atmosphere; Microwave irradiation;

DOI:10.1039/c2cc36275a

Reference yield:

1,2-dimethoxy-3,6-dimethyl-4,5-dinitrobenzene (1333889-84-1) → C28H52N2O8Si2 (1409937-10-5)

Guidance literature:

Multi-step reaction with 2 steps

1: boron tribromide / dichloromethane / 16 h / 50 °C / Inert atmosphere

2: cyanomethylenetributyl-phosphorane / tetrahydrofuran / 24 h / 80 °C / Inert atmosphere; Microwave irradiation

With boron tribromide; cyanomethylenetributyl-phosphorane; In tetrahydrofuran; dichloromethane;

DOI:10.1039/c2cc36275a

Reference yield:

C28H52N2O8Si2 (1409937-10-5) → C42H62N2O4Si2

Guidance literature:

Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 27 h

2: acetic acid / toluene / 17 h / 120 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; acetic acid; In ethanol; toluene;

DOI:10.1039/c2cc36275a

upstream raw materials:

3,6-dimethyl-4,5-dinitrobenzene-1,2-diol

(R)-3-(tert-butyldimethylsilyloxy)-2-methylpropan-1-ol

1,2-dimethoxy-3,6-dimethyl-4,5-dinitrobenzene

Downstream raw materials:

C₃₀H₅₂N₂O₄Si₂