(R)-hexan-3-yl benzoate

Base Information

Chemical Name:(R)-hexan-3-yl benzoate
CAS No.:1384266-66-3
Molecular Formula:C₁₃H₁₈O₂
Molecular Weight:206.285
Hs Code.:

Synonyms:(R)-hexan-3-yl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-hexan-3-yl benzoate

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Technology Process of (R)-hexan-3-yl benzoate

There total 6 articles about (R)-hexan-3-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 80155-86-8
(Z)-1-ethylbut-1-enyl benzoate

: 1384266-66-3
(R)-hexan-3-yl benzoate

Guidance literature:: With C₄₉H₅₄O₃P₂Rh⁽¹⁺⁾*BF₄^(1-); hydrogen; In 1,2-dichloro-ethane; at 40 ℃; for 24h; under 3000.3 Torr; enantioselective reaction; Inert atmosphere; Glovebox;
DOI:10.1021/acs.joc.7b00710

Reference yield:

: hex-2-en-3-yl benzoate

: 1384266-66-3
(R)-hexan-3-yl benzoate

: (S)-hexan-3-yl benzoate

Guidance literature:: With bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; 4-[5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy]-3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']dinaphthalene; In dichloromethane; at 30 ℃; for 20h; under 45004.5 Torr; optical yield given as %ee; Inert atmosphere; Autoclave;
DOI:10.1021/ol301563g

Reference yield:

: 1-bromopropyl benzoate

: 187737-37-7,13987-01-4,15220-87-8,9003-07-0,676-63-1,25085-53-4
propene

: 1384266-66-3
(R)-hexan-3-yl benzoate

: (S)-hexan-3-yl benzoate

Guidance literature:: With potassium phosphate monohydrate; Triethoxysilane; nickel(II) bromide 2-methoxyethyl ether complex; C₄₅H₃₈N₂O₂; In tert-butyl methyl ether; at -77 - 20 ℃; Overall yield = 79 percent; Overall yield = 130 mg; enantioselective reaction; Inert atmosphere; Sealed tube; Schlenk technique;
DOI:10.1021/jacs.0c01324