4-(4-fluorophenyl)-3,4,5,6-tetrahydrobenzo[h]quinazoline-2(1H)-thione

Base Information

Chemical Name:4-(4-fluorophenyl)-3,4,5,6-tetrahydrobenzo[h]quinazoline-2(1H)-thione
CAS No.:128483-25-0
Molecular Formula:C₁₈H₁₅FN₂S
Molecular Weight:310.395
Hs Code.:
Mol file:128483-25-0.mol

Synonyms:2-Mercapto-4-p-fluorophenyl-4H-1,2,3,4,5,6-hexahydrobenzo-quinazoline

Suppliers and Price of 4-(4-fluorophenyl)-3,4,5,6-tetrahydrobenzo[h]quinazoline-2(1H)-thione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4-fluorophenyl)-3,4,5,6-tetrahydrobenzo[h]quinazoline-2(1H)-thione

Chemical Property:

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Technology Process of 4-(4-fluorophenyl)-3,4,5,6-tetrahydrobenzo[h]quinazoline-2(1H)-thione

There total 4 articles about 4-(4-fluorophenyl)-3,4,5,6-tetrahydrobenzo[h]quinazoline-2(1H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 459-57-4
4-fluorobenzaldehyde

: 17356-08-0
thiourea

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 128483-25-0
2-Mercapto-4-p-fluorophenyl-4H-1,2,3,4,5,6-hexahydrobenzo-quinazoline

Guidance literature:: With poly(4-vinylpyridinium)hydrogen sulfate; In neat (no solvent); at 120 ℃;
DOI:10.1039/c4ra02514h

Reference yield: 83.0%

: 59082-25-6,59082-37-0,66045-89-4
2-(4-fluorobenzylidene)-3,4-dihydronaphthalen-1(2H)-one

: 17356-08-0
thiourea

: 128483-25-0
2-Mercapto-4-p-fluorophenyl-4H-1,2,3,4,5,6-hexahydrobenzo-quinazoline

Guidance literature:: With potassium hydroxide; In ethanol; for 0.5h; Heating;

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 128483-25-0
2-Mercapto-4-p-fluorophenyl-4H-1,2,3,4,5,6-hexahydrobenzo-quinazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 4percent KOH / ethanol / 0.08 h / Ambient temperature

2: 83 percent / aq. KOH / ethanol / 0.5 h / Heating

With potassium hydroxide; In ethanol;