[7α,8α,3',4']-N'-[4-(bromobutoxy)phenethyl]succinimido-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine

Base Information

• Chemical Name: [7α,8α,3',4']-N'-[4-(bromobutoxy)phenethyl]succinimido-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine
• CAS No.: 904315-39-5
• Molecular Formula: C₃₅H₃₉BrN₂O₆
• Molecular Weight: 663.608

Synonyms:[7α,8α,3',4']-N'-[4-(bromobutoxy)phenethyl]succinimido-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine

Chemical Property of [7α,8α,3',4']-N'-[4-(bromobutoxy)phenethyl]succinimido-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine

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Technology Process of [7α,8α,3',4']-N'-[4-(bromobutoxy)phenethyl]succinimido-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine

There total 1 articles about [7α,8α,3',4']-N'-[4-(bromobutoxy)phenethyl]succinimido-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C31H32N2O6 (904315-33-9) + 1,4-dibromo-butane (110-52-1) → [7α,8α,3',4']-N'-[4-(bromobutoxy)phenethyl]succinimido-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine (904315-39-5)

Guidance literature:

With sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; water; at 20 ℃; for 24h;

DOI:10.1007/s11178-005-0306-8

Reference yield: 85.0%

[7α,8α,3',4']-N'-[4-(bromobutoxy)phenethyl]succinimido-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine (904315-39-5) → C35H43BrN2O4

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; Heating;

DOI:10.1007/s11178-005-0306-8

Reference yield: 29.0%

[7α,8α,3',4']-N'-[4-(bromobutoxy)phenethyl]succinimido-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine (904315-39-5) + ethanolamine (141-43-5) → [7α,8α,3',4']-N'-{4-[4-(2-aminoethoxy)butoxy]phenethyl}succinimido-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine + [7α,8α,3',4']-N'-{4-[4-(2-hydroxyethylamino)butoxy]phenethyl}succinimido-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine

Guidance literature:

With potassium carbonate; In acetone; for 8h; Heating;

DOI:10.1007/s11178-005-0306-8

upstream raw materials:

C₃₁H₃₂N₂O₆

1,4-dibromo-butane

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