3-Chloropropyl 4-Methoxyphenyl Ether

Base Information

• Chemical Name: 3-Chloropropyl 4-Methoxyphenyl Ether
• CAS No.: 20744-03-0
• Molecular Formula: C₁₀H₁₃ClO₂
• Molecular Weight: 200.665
• Mol file: 20744-03-0.mol

Synonyms:1-(3-chloropropoxy)-4-methoxybenzene

Chemical Property of 3-Chloropropyl 4-Methoxyphenyl Ether

Chemical Property:

• Storage Temp.: -20°C Freezer
• Solubility.: Dichloromethane, Dimethylsulfoxide, Ethyl Acetate, Methanol, Hexanes

Purity/Quality:

99% ^*data from raw suppliers

3-Chloropropyl4-MethoxyphenylEther ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 3-Chloropropyl 4-methoxyphenyl Ether is a reactant used in the preparation of antimycotic imidazoles, antipsychotic agents and piperidines with antihistaminic activity.

Technology Process of 3-Chloropropyl 4-Methoxyphenyl Ether

There total 5 articles about 3-Chloropropyl 4-Methoxyphenyl Ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-methoxy-phenol (150-76-5) + 1-chloro-3-hydroxypropane (627-30-5) → 1-(3-chloropropoxy)-4-methoxybenzene (20744-03-0)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In dichloromethane; at 0 - 20 ℃; for 72.5h;

Reference yield: 88.0%

3-chloropropyl p-toluenesulfonate (632-02-0) + 4-methoxy-phenol (150-76-5) → 1,3-bis(4-methoxyphenoxy)propane (3875-75-0) + 1-(3-chloropropoxy)-4-methoxybenzene (20744-03-0)

Guidance literature:

With potassium carbonate; In acetonitrile; for 17.5h; Reflux; Inert atmosphere;

DOI:10.1007/s11172-017-1732-9

Reference yield: 82.0%

4-methoxy-phenol (150-76-5) + 1.3-chlorobromopropane (109-70-6) → 1-(3-chloropropoxy)-4-methoxybenzene (20744-03-0)

Guidance literature:

With potassium carbonate; In acetone; for 24h; Heating;

DOI:10.1021/jm00121a022

upstream raw materials:

4-methoxy-phenol

1.3-chlorobromopropane

1-chloro-3-hydroxypropane

3-chloropropyl p-toluenesulfonate

Downstream raw materials:

4-[bis(4-fluorophenyl)methyl]-1-[3-(4-methoxyphenoxy)propyl]piperidine

α,α-Bis(4-fluorophenyl)-1-[3-(4-methoxyphenoxy)propyl]-4-piperidine-methanol

2-(2,4-Dichloro-phenyl)-5-(4-methoxy-phenoxy)-pentanenitrile

N-<3-(4-Methoxy-phenoxy)-propyl>-anilin

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