1,3,5-Triallyl-5-<1-(2-methoxyphenyl)-2-phenylethyl>-2,4,6-trioxohexahydropyrimidine

Base Information

Chemical Name:1,3,5-Triallyl-5-<1-(2-methoxyphenyl)-2-phenylethyl>-2,4,6-trioxohexahydropyrimidine
CAS No.:109317-92-2
Molecular Formula:C₂₈H₃₀N₂O₄
Molecular Weight:458.557
Hs Code.:

Synonyms:1,3,5-Triallyl-5-<1-(2-methoxyphenyl)-2-phenylethyl>-2,4,6-trioxohexahydropyrimidine

Suppliers and Price of 1,3,5-Triallyl-5-<1-(2-methoxyphenyl)-2-phenylethyl>-2,4,6-trioxohexahydropyrimidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 1,3,5-Triallyl-5-<1-(2-methoxyphenyl)-2-phenylethyl>-2,4,6-trioxohexahydropyrimidine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of 1,3,5-Triallyl-5-<1-(2-methoxyphenyl)-2-phenylethyl>-2,4,6-trioxohexahydropyrimidine

There total 3 articles about 1,3,5-Triallyl-5-<1-(2-methoxyphenyl)-2-phenylethyl>-2,4,6-trioxohexahydropyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 109317-87-5
5-<1-(2-Methoxyphenyl)-2-phenylethyl>-barbituric acid

: 106-95-6
allyl bromide

: 109317-92-2
1,3,5-Triallyl-5-<1-(2-methoxyphenyl)-2-phenylethyl>-2,4,6-trioxohexahydropyrimidine

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; for 48h; Ambient temperature;
DOI:10.1055/s-1986-31870

Reference yield:

: 62673-31-8
benzyl(bromo)zinc

: 109317-92-2
1,3,5-Triallyl-5-<1-(2-methoxyphenyl)-2-phenylethyl>-2,4,6-trioxohexahydropyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / tetrahydrofuran / 1 h / Ambient temperature

2: 50 percent / aq. NaOH / benzyltriethylammonium chloride / CH₂Cl₂ / 48 h / Ambient temperature

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-1986-31870

Reference yield:

: 23450-43-3
5-<(2-Methoxyphenyl)methylene>-2,4,6(1H,3H)-pyrimidinetrione

: 109317-92-2
1,3,5-Triallyl-5-<1-(2-methoxyphenyl)-2-phenylethyl>-2,4,6-trioxohexahydropyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / tetrahydrofuran / 1 h / Ambient temperature

2: 50 percent / aq. NaOH / benzyltriethylammonium chloride / CH₂Cl₂ / 48 h / Ambient temperature

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-1986-31870