(E)-3-(4-Benzyloxy-phenyl)-1-(5-chloro-2-hydroxy-3-methyl-phenyl)-propenone

Base Information

Chemical Name:(E)-3-(4-Benzyloxy-phenyl)-1-(5-chloro-2-hydroxy-3-methyl-phenyl)-propenone
CAS No.:111391-47-0
Molecular Formula:C₂₃H₁₉ClO₃
Molecular Weight:378.855
Hs Code.:

Synonyms:(E)-3-(4-Benzyloxy-phenyl)-1-(5-chloro-2-hydroxy-3-methyl-phenyl)-propenone

Suppliers and Price of (E)-3-(4-Benzyloxy-phenyl)-1-(5-chloro-2-hydroxy-3-methyl-phenyl)-propenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(4-Benzyloxy-phenyl)-1-(5-chloro-2-hydroxy-3-methyl-phenyl)-propenone

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Technology Process of (E)-3-(4-Benzyloxy-phenyl)-1-(5-chloro-2-hydroxy-3-methyl-phenyl)-propenone

There total 1 articles about (E)-3-(4-Benzyloxy-phenyl)-1-(5-chloro-2-hydroxy-3-methyl-phenyl)-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 4397-53-9
p-benzyloxybenzaldehyde

: 50343-12-9
1-(5-chloro-2-hydroxy-3-methylphenyl)ethanone

: 111391-47-0
(E)-3-(4-Benzyloxy-phenyl)-1-(5-chloro-2-hydroxy-3-methyl-phenyl)-propenone

Guidance literature:: With sodium hydroxide; In ethanol; for 48h; Ambient temperature;
DOI:10.1021/jm00106a039

Reference yield: 50.0%

: 111391-47-0
(E)-3-(4-Benzyloxy-phenyl)-1-(5-chloro-2-hydroxy-3-methyl-phenyl)-propenone

: 111391-60-7
2-(4-Benzyloxy-phenyl)-6-chloro-3-hydroxy-8-methyl-chromen-4-one

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; In methanol; for 0.25h;
DOI:10.1021/jm00106a039

Reference yield:

: 111391-47-0
(E)-3-(4-Benzyloxy-phenyl)-1-(5-chloro-2-hydroxy-3-methyl-phenyl)-propenone

: 111391-90-3
6-Chloro-2-(4-hydroxy-phenyl)-3-methoxy-8-methyl-chromen-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / 10percent NaOH, 30percent H₂O₂ / methanol / 0.25 h

2: 92 percent / K₂CO₃ / acetone / 16 h / Heating

3: 57 percent / AcOH, HCl / 3 h / Heating

With hydrogenchloride; sodium hydroxide; dihydrogen peroxide; potassium carbonate; acetic acid; In methanol; acetone;
DOI:10.1021/jm00106a039