C₃₂H₃₄NO₁₁P

Base Information

Chemical Name:C₃₂H₃₄NO₁₁P
CAS No.:87462-01-9
Molecular Formula:C₃₂H₃₄NO₁₁P
Molecular Weight:639.596
Hs Code.:

C<sub>32</sub>H<sub>34</sub>NO<sub>11</sub>P

Synonyms:C₃₂H₃₄NO₁₁P

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Chemical Property of C₃₂H₃₄NO₁₁P

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Technology Process of C₃₂H₃₄NO₁₁P

There total 15 articles about C₃₂H₃₄NO₁₁P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-88-4
benzoyl chloride

: 87462-01-9
C₃₂H₃₄NO₁₁P

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) NaBH₄, CeCl₃*7H₂O / 1.) ethanol, methanol, -78 deg C

2: 1.) m-chloroperbenzoic acid

3: 92 percent / aq. N-bromosuccinimide, aq. AcOH / CH₂Cl₂

4: 96 percent / DBN

5: 1.) tetra-n-butylammonium azide, trimethylsilyl azide, 2.) TFA / 2.) MeOH

6: 1.) NaH, 2.) K₂CO₃, MeOH

With methanol; sodium tetrahydroborate; N-Bromosuccinimide; cerium(III) chloride; trimethylsilylazide; 2,6-dichloro-benzonitrile; tetrabutylammoniun azide; sodium hydride; potassium carbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/ja00360a030

Reference yield:

: 87461-99-2
C₃₀H₂₉BrO₉

: 87462-01-9
C₃₂H₃₄NO₁₁P

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / 1,5-diazabicyclo<4.3.0>non-5-ene (DBN) / benzene / 1 h / 25 °C

2: toluene / 10 h / 90 °C

3: trifluoroacetic acid / CH₂Cl₂; methanol / 1 h

4: 90 percent / triethylamine (Et₃N) / CH₂Cl₂ / 3.5 h / 0 °C

5: 2.) sodium hydride / 1.) benzene, 25 deg C, 20 h; 2.) THF, 25 deg C, 3 h

With DBN; sodium hydride; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; toluene; benzene;
DOI:10.1021/ja00291a029

Reference yield:

: 87461-97-0
C₃₀H₂₈O₈

: 87462-01-9
C₃₂H₃₄NO₁₁P

Guidance literature:: Multi-step reaction with 6 steps

1: 92 percent / N-bromosuccinimide (NBS), H₂O, acetic acid / CH₂Cl₂ / 5 h / 25 °C

2: 96 percent / 1,5-diazabicyclo<4.3.0>non-5-ene (DBN) / benzene / 1 h / 25 °C

3: toluene / 10 h / 90 °C

4: trifluoroacetic acid / CH₂Cl₂; methanol / 1 h

5: 90 percent / triethylamine (Et₃N) / CH₂Cl₂ / 3.5 h / 0 °C

6: 2.) sodium hydride / 1.) benzene, 25 deg C, 20 h; 2.) THF, 25 deg C, 3 h

With N-Bromosuccinimide; DBN; water; sodium hydride; acetic acid; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; toluene; benzene;
DOI:10.1021/ja00291a029