2,3-Dideuteriocyclohexanone

Base Information

• Chemical Name: 2,3-Dideuteriocyclohexanone
• CAS No.: 120625-93-6
• Molecular Formula: C₆H₁₀O
• Molecular Weight: 100.129
• Mol file: 120625-93-6.mol

Synonyms:2,3-Dideuteriocyclohexanone

Chemical Property of 2,3-Dideuteriocyclohexanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-Dideuteriocyclohexanone

There total 2 articles about 2,3-Dideuteriocyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexenone (930-68-7) → 1,2,3-Trideuteriocyclohexanol-O-d (123438-31-3) + 2,3-Dideuteriocyclohexanone (120625-93-6)

Guidance literature:

With deuterium; hydrido(triphenylphosphine)copper(I) hexamer; copper; triphenylphosphine; In benzene-d6; for 52h; under 18100.2 Torr; Ambient temperature;

DOI:10.1021/ja00206a008

Reference yield:

cyclohexenone (930-68-7) → 2,3-Dideuteriocyclohexanone (120625-93-6)

Guidance literature:

With deuterium; Wilkinson's catalyst;

DOI:10.1021/ja00415a048

Reference yield:

2,3-Dideuteriocyclohexanone (120625-93-6) → cyclohexanone-3-d (72194-82-2)

Guidance literature:

With sodium hydrogencarbonate;

DOI:10.1021/ja00415a048

upstream raw materials:

cyclohexenone

Downstream raw materials:

cyclohexanone-3-d