(S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propionaldehyde

Base Information

Chemical Name:(S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propionaldehyde
CAS No.:150824-13-8
Molecular Formula:C₁₈H₃₀O₄SSi
Molecular Weight:370.585
Hs Code.:

Synonyms:(S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propionaldehyde

Suppliers and Price of (S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propionaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propionaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propionaldehyde

There total 5 articles about (S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1541-10-2
mesitylthiol

: 150824-13-8
(S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propionaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: NaH / tetrahydrofuran / 1.) 30 min

2: 30percent H₂O₂ / acetic acid

3: DMAP / CH₂Cl₂

4: HCOOH / 10percent Pd/C / ethanol

5: 1. ) (COCl)2, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, -63 deg C, 30 min

With dmap; formic acid; oxalyl dichloride; dihydrogen peroxide; sodium hydride; dimethyl sulfoxide; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; acetic acid;
DOI:10.1021/jo00074a045

Reference yield:

: 150824-10-5
(S)-1-O-Benzyl-3-(mesitylthio)-1,2-propanediol

: 150824-13-8
(S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propionaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 30percent H₂O₂ / acetic acid

2: DMAP / CH₂Cl₂

3: HCOOH / 10percent Pd/C / ethanol

4: 1. ) (COCl)2, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, -63 deg C, 30 min

With dmap; formic acid; oxalyl dichloride; dihydrogen peroxide; dimethyl sulfoxide; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid;
DOI:10.1021/jo00074a045

Reference yield:

: 150824-11-6
(S)-1-Benzyloxy-3-(2,4,6-trimethyl-benzenesulfonyl)-propan-2-ol

: 150824-13-8
(S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propionaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: DMAP / CH₂Cl₂

2: HCOOH / 10percent Pd/C / ethanol

3: 1. ) (COCl)2, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, -63 deg C, 30 min

With dmap; formic acid; oxalyl dichloride; dimethyl sulfoxide; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jo00074a045