(S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propan-1-ol

Base Information

Chemical Name:(S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propan-1-ol
CAS No.:150824-12-7
Molecular Formula:C₁₈H₃₂O₄SSi
Molecular Weight:372.601
Hs Code.:

Synonyms:(S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propan-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propan-1-ol

Chemical Property:

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Technology Process of (S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propan-1-ol

There total 4 articles about (S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [(S)-1-Benzyloxymethyl-2-(2,4,6-trimethyl-benzenesulfonyl)-ethoxy]-tert-butyl-dimethyl-silane

: 150824-12-7
(S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propan-1-ol

Guidance literature:: With formic acid; palladium on activated charcoal; In ethanol;
DOI:10.1021/jo00074a045

Reference yield:

: 1541-10-2
mesitylthiol

: 150824-12-7
(S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / tetrahydrofuran / 1.) 30 min

2: 30percent H₂O₂ / acetic acid

3: DMAP / CH₂Cl₂

4: HCOOH / 10percent Pd/C / ethanol

With dmap; formic acid; dihydrogen peroxide; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; acetic acid;
DOI:10.1021/jo00074a045

Reference yield:

: 150824-10-5
(S)-1-O-Benzyl-3-(mesitylthio)-1,2-propanediol

: 150824-12-7
(S)-2-(tert-Butyl-dimethyl-silanyloxy)-3-(2,4,6-trimethyl-benzenesulfonyl)-propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 30percent H₂O₂ / acetic acid

2: DMAP / CH₂Cl₂

3: HCOOH / 10percent Pd/C / ethanol

With dmap; formic acid; dihydrogen peroxide; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid;
DOI:10.1021/jo00074a045