4-(2-hydroxyacetyl)phenyl acetate

Base Information

Chemical Name:4-(2-hydroxyacetyl)phenyl acetate
CAS No.:52728-03-7
Molecular Formula:C₁₀H₁₀O₄
Molecular Weight:194.187
Hs Code.:

Synonyms:4-(2-hydroxyacetyl)phenyl acetate

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Chemical Property of 4-(2-hydroxyacetyl)phenyl acetate

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 4-(2-hydroxyacetyl)phenyl acetate

There total 7 articles about 4-(2-hydroxyacetyl)phenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 2628-16-2
p-acetoxystyrene

: 52728-03-7
4-(2-hydroxyacetyl)phenyl acetate

Guidance literature:: With 4,5-Diazafluoren-9-one; dihydrogen peroxide; palladium diacetate; trifluoroacetic acid; In tetrahydrofuran; water; at 75 ℃; for 6h; Sealed tube; Green chemistry;
DOI:10.1021/acs.orglett.7b01228

Reference yield: 62.0%

: 86941-88-0
Acetic acid 4-(1-trimethylsilanyloxy-vinyl)-phenyl ester

: 52728-03-7
4-(2-hydroxyacetyl)phenyl acetate

Guidance literature:: Acetic acid 4-(1-trimethylsilanyloxy-vinyl)-phenyl ester; With magnesium sulfate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -20 ℃; for 4h; Inert atmosphere;

With citric acid; In methanol; dichloromethane; water; at 20 ℃; for 0.166667h;
DOI:10.1039/c9cc07943b

Reference yield:

: 13031-43-1
4-acetyloxyacetophenone

: 52728-03-7
4-(2-hydroxyacetyl)phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / dimethylformamide / 85 °C

2: 1.) 3-chloroperbenzoic acid; 2.) citric acid / 1.) CH₂Cl₂; 2.) MeOH

With triethylamine; 3-chloro-benzenecarboperoxoic acid; citric acid; In N,N-dimethyl-formamide;
DOI:10.1002/hlca.19940770616