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(-)-methyl 4-epi-quinate

Base Information
  • Chemical Name:(-)-methyl 4-epi-quinate
  • CAS No.:50459-25-1
  • Molecular Formula:C8H14O6
  • Molecular Weight:206.196
  • Hs Code.:
(-)-methyl 4-epi-quinate

Synonyms:(-)-methyl 4-epi-quinate

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Chemical Property of (-)-methyl 4-epi-quinate
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Technology Process of (-)-methyl 4-epi-quinate

There total 7 articles about (-)-methyl 4-epi-quinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 4 steps
1: Dess-Martin periodane / dichloromethane / 20 °C
2: sodium tetrahydroborate / ethanol / 0.67 h / -30 °C
3: hydrogenchloride / water / 1 h
4: Amberlite IR120 acidic resin / 12 h
With hydrogenchloride; sodium tetrahydroborate; Dess-Martin periodane; In ethanol; dichloromethane; water;
DOI:10.1021/acs.jafc.6b02472
Guidance literature:
Multi-step reaction with 6 steps
1: Amberlite IR120 acidic resin / 12 h / Reflux
2: triethylamine / N,N-dimethyl-formamide / 18 h / 0 - 20 °C / Inert atmosphere
3: Dess-Martin periodane / dichloromethane / 20 °C
4: sodium tetrahydroborate / ethanol / 0.67 h / -30 °C
5: hydrogenchloride / water / 1 h
6: Amberlite IR120 acidic resin / 12 h
With hydrogenchloride; sodium tetrahydroborate; Dess-Martin periodane; triethylamine; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/acs.jafc.6b02472
Guidance literature:
Multi-step reaction with 2 steps
1: hydrogenchloride / water / 1 h
2: Amberlite IR120 acidic resin / 12 h
With hydrogenchloride; In water;
DOI:10.1021/acs.jafc.6b02472
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