n,N'-(naphthalene-2,6-diylbis(2,1-phenylene))bis(dodecane-1-sulfonamide)

Base Information

Chemical Name:n,N'-(naphthalene-2,6-diylbis(2,1-phenylene))bis(dodecane-1-sulfonamide)
CAS No.:1380244-98-3
Molecular Formula:C₄₆H₆₆N₂O₄S₂
Molecular Weight:775.173
Hs Code.:

Synonyms:n,N'-(naphthalene-2,6-diylbis(2,1-phenylene))bis(dodecane-1-sulfonamide)

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Chemical Property of n,N'-(naphthalene-2,6-diylbis(2,1-phenylene))bis(dodecane-1-sulfonamide)

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Technology Process of n,N'-(naphthalene-2,6-diylbis(2,1-phenylene))bis(dodecane-1-sulfonamide)

There total 4 articles about n,N'-(naphthalene-2,6-diylbis(2,1-phenylene))bis(dodecane-1-sulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 1380244-84-7
N-(2-bromophenyl)dodecane-1-sulfonamide

: 1380244-95-0
2,6-bis(tributylstannyl)naphthalene

: 1380244-98-3
n,N'-(naphthalene-2,6-diylbis(2,1-phenylene))bis(dodecane-1-sulfonamide)

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 120 ℃; for 72h; Inert atmosphere; Sealed vessel;

Reference yield:

: 13720-06-4
2,6-dibromonaphthalene

: 1380244-98-3
n,N'-(naphthalene-2,6-diylbis(2,1-phenylene))bis(dodecane-1-sulfonamide)

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium / diethyl ether; pentane / 18 h / -78 - 23 °C / Inert atmosphere

1.2: 5 h / -78 - 23 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 72 h / 120 °C / Inert atmosphere; Sealed vessel

With tert.-butyl lithium; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In diethyl ether; toluene; pentane;

Reference yield:

: 10147-40-7
1-Dodecanesulfonyl chloride

: 1380244-98-3
n,N'-(naphthalene-2,6-diylbis(2,1-phenylene))bis(dodecane-1-sulfonamide)

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dmap / 72 h / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 72 h / 120 °C / Inert atmosphere; Sealed vessel

With pyridine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene;