C₅₄H₇₄O₄

Base Information

Chemical Name:C₅₄H₇₄O₄
CAS No.:186772-50-9
Molecular Formula:C₅₄H₇₄O₄
Molecular Weight:787.179
Hs Code.:

C<sub>54</sub>H<sub>74</sub>O<sub>4</sub>

Synonyms:C₅₄H₇₄O₄

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Chemical Property of C₅₄H₇₄O₄

Chemical Property:

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Technology Process of C₅₄H₇₄O₄

There total 12 articles about C₅₄H₇₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 437706-92-8
C₇₂H₁₁₄O₄Si₂

: 186772-50-9
C₅₄H₇₄O₄

: 437707-01-2
C₆₃H₉₄O₄Si

Guidance literature:: With tetrabutyl ammonium fluoride; water; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1021/ja012458m

Reference yield:

: 7149-03-3
ethyl 3-bromo-4-aminobenzoate

: 186772-50-9
C₅₄H₇₄O₄

Guidance literature:: Multi-step reaction with 8 steps

1: 94 percent / ICl / acetic acid; H₂O / 10 h / 80 °C

2: 88 percent / NaNO₂; H₂SO₄ / benzene; ethanol / 1.5 h / Heating

3: 99 percent / Pd₂(dba)3*CHCl₃; triphenylphosphine; triethylamine / CuI / 36 h

4: 92 percent / Pd₂(dba)3*CHCl₃; triphenylphosphine; triethylamine / CuI / 16 h

5: 97 percent / KOH / tetrahydrofuran; H₂O / 71 h / 20 °C

6: 91 percent / DMAP; DCC / 1,2-dichloro-ethane / 4 h / 20 °C

7: 96 percent / Cu(OAc)2; pyridine / 4 h / 20 °C

8: 22 percent / TBAF; water / tetrahydrofuran / 4 h / 20 °C

With pyridine; dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium hydroxide; copper diacetate; sulfuric acid; tetrabutyl ammonium fluoride; water; Iodine monochloride; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; sodium nitrite; copper(l) iodide; In tetrahydrofuran; ethanol; water; acetic acid; 1,2-dichloro-ethane; benzene;
DOI:10.1021/ja012458m

Reference yield:

: 94-09-7
p-aminoethylbenzoate

: 186772-50-9
C₅₄H₇₄O₄

Guidance literature:: Multi-step reaction with 9 steps

1: 99 percent / N-bromosuccinimide / CHCl₃ / 4 h / 5 - 10 °C

2: 94 percent / ICl / acetic acid; H₂O / 10 h / 80 °C

3: 88 percent / NaNO₂; H₂SO₄ / benzene; ethanol / 1.5 h / Heating

4: 99 percent / Pd₂(dba)3*CHCl₃; triphenylphosphine; triethylamine / CuI / 36 h

5: 92 percent / Pd₂(dba)3*CHCl₃; triphenylphosphine; triethylamine / CuI / 16 h

6: 97 percent / KOH / tetrahydrofuran; H₂O / 71 h / 20 °C

7: 91 percent / DMAP; DCC / 1,2-dichloro-ethane / 4 h / 20 °C

8: 96 percent / Cu(OAc)2; pyridine / 4 h / 20 °C

9: 22 percent / TBAF; water / tetrahydrofuran / 4 h / 20 °C

With pyridine; dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium hydroxide; N-Bromosuccinimide; copper diacetate; sulfuric acid; tetrabutyl ammonium fluoride; water; Iodine monochloride; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; sodium nitrite; copper(l) iodide; In tetrahydrofuran; ethanol; chloroform; water; acetic acid; 1,2-dichloro-ethane; benzene;
DOI:10.1021/ja012458m