5,5'-(5-nitro-1,3-phenylene)bis(3-(3,4-bis(dodecyloxy)phenyl)-1,2,4-oxadiazole)

Base Information

Chemical Name:5,5'-(5-nitro-1,3-phenylene)bis(3-(3,4-bis(dodecyloxy)phenyl)-1,2,4-oxadiazole)
CAS No.:1349701-90-1
Molecular Formula:C₇₀H₁₀₉N₅O₈
Molecular Weight:1148.66
Hs Code.:

Synonyms:5,5'-(5-nitro-1,3-phenylene)bis(3-(3,4-bis(dodecyloxy)phenyl)-1,2,4-oxadiazole)

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Chemical Property of 5,5'-(5-nitro-1,3-phenylene)bis(3-(3,4-bis(dodecyloxy)phenyl)-1,2,4-oxadiazole)

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Technology Process of 5,5'-(5-nitro-1,3-phenylene)bis(3-(3,4-bis(dodecyloxy)phenyl)-1,2,4-oxadiazole)

There total 5 articles about 5,5'-(5-nitro-1,3-phenylene)bis(3-(3,4-bis(dodecyloxy)phenyl)-1,2,4-oxadiazole) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13438-30-7
5-nitro-1,3-benzenedicarbonylchloride

: 1349701-84-3
3,4-bis(dodecyloxy)-N'-hydroxybenzimidamide

: 1349701-90-1
5,5'-(5-nitro-1,3-phenylene)bis(3-(3,4-bis(dodecyloxy)phenyl)-1,2,4-oxadiazole)

Guidance literature:: With pyridine; for 24h; Reflux;
DOI:10.1016/j.tet.2011.10.019

Reference yield:

: 17345-61-8
3,4-dihydroxybenzonitrile

: 1349701-90-1
5,5'-(5-nitro-1,3-phenylene)bis(3-(3,4-bis(dodecyloxy)phenyl)-1,2,4-oxadiazole)

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylammomium bromide; potassium carbonate / butanone / 24 h / Reflux

2: hydroxylamine hydrochloride; potassium hydroxide / methanol; water / 24 h / Reflux

3: pyridine / 24 h / Reflux

With pyridine; hydroxylamine hydrochloride; tetrabutylammomium bromide; potassium carbonate; potassium hydroxide; In methanol; water; butanone; 2: Thiemann reaction;
DOI:10.1016/j.tet.2011.10.019

Reference yield:

: 405549-76-0
3,4-bis(dodecyloxy)benzonitrile

: 1349701-90-1
5,5'-(5-nitro-1,3-phenylene)bis(3-(3,4-bis(dodecyloxy)phenyl)-1,2,4-oxadiazole)

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; potassium hydroxide / methanol; water / 24 h / Reflux

2: pyridine / 24 h / Reflux

With pyridine; hydroxylamine hydrochloride; potassium hydroxide; In methanol; water; 1: Thiemann reaction;
DOI:10.1016/j.tet.2011.10.019