1,9-dimethyl-17-benzyl-1,9,17-triaza<2.2.2>metacyclophane-2,10,18-trione

Base Information

Chemical Name:1,9-dimethyl-17-benzyl-1,9,17-triaza<2.2.2>metacyclophane-2,10,18-trione
CAS No.:77149-39-4
Molecular Formula:C₃₀H₂₅N₃O₃
Molecular Weight:475.547
Hs Code.:

Synonyms:1,9-dimethyl-17-benzyl-1,9,17-triaza<2.2.2>metacyclophane-2,10,18-trione

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Chemical Property of 1,9-dimethyl-17-benzyl-1,9,17-triaza<2.2.2>metacyclophane-2,10,18-trione

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Technology Process of 1,9-dimethyl-17-benzyl-1,9,17-triaza<2.2.2>metacyclophane-2,10,18-trione

There total 7 articles about 1,9-dimethyl-17-benzyl-1,9,17-triaza<2.2.2>metacyclophane-2,10,18-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 100-39-0
benzyl bromide

: 77149-38-3
1,9-dimethyl-1,9,17-triaza<2.2.2>metacyclophane-2,10,18-trione

: 77149-39-4
1,9-dimethyl-17-benzyl-1,9,17-triaza<2.2.2>metacyclophane-2,10,18-trione

Guidance literature:: With sodium hydride; In tetrahydrofuran; Ambient temperature;
DOI:10.1039/P19820001727

Reference yield:

: 77149-33-8
3-[Methyl-(3-nitro-benzoyl)-amino]-benzoyl chloride

: 77149-39-4
1,9-dimethyl-17-benzyl-1,9,17-triaza<2.2.2>metacyclophane-2,10,18-trione

Guidance literature:: Multi-step reaction with 6 steps

1: NaOH / aq. ethanol

2: NaH / dimethylsulfoxide

3: KOH / dimethylsulfoxide; H₂O

4: H₂ / PtO₂ / ethanol

5: 26 percent / N,N'-dicyclohexylcarbodiimide / CH₂Cl₂

6: NaH / tetrahydrofuran

With potassium hydroxide; sodium hydroxide; hydrogen; sodium hydride; dicyclohexyl-carbodiimide; platinum(IV) oxide; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(00)93692-X

Reference yield:

: 77149-32-7
3-(N-methyl-3-nitrobenzamido)benzoic acid

: 77149-39-4
1,9-dimethyl-17-benzyl-1,9,17-triaza<2.2.2>metacyclophane-2,10,18-trione

Guidance literature:: Multi-step reaction with 7 steps

1: SOCl₂

2: NaOH / aq. ethanol

3: NaH / dimethylsulfoxide

4: KOH / dimethylsulfoxide; H₂O

5: H₂ / PtO₂ / ethanol

6: 26 percent / N,N'-dicyclohexylcarbodiimide / CH₂Cl₂

7: NaH / tetrahydrofuran

With potassium hydroxide; sodium hydroxide; thionyl chloride; hydrogen; sodium hydride; dicyclohexyl-carbodiimide; platinum(IV) oxide; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(00)93692-X