N,N''-bis[3-benzyloxy-1-carbamidomethyl-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl(2-mercaptothiazolide)]-N'-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]-bis(2-aminoethyl)amine

Base Information

Chemical Name:N,N''-bis[3-benzyloxy-1-carbamidomethyl-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl(2-mercaptothiazolide)]-N'-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]-bis(2-aminoethyl)amine
CAS No.:1610625-74-5
Molecular Formula:C₄₉H₅₉N₇O₁₁S₄
Molecular Weight:1050.31
Hs Code.:

N,N''-bis[3-benzyloxy-1-carbamidomethyl-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl(2-mercaptothiazolide)]-N'-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]-bis(2-aminoethyl)amine

Synonyms:N,N''-bis[3-benzyloxy-1-carbamidomethyl-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl(2-mercaptothiazolide)]-N'-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]-bis(2-aminoethyl)amine

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Chemical Property of N,N''-bis[3-benzyloxy-1-carbamidomethyl-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl(2-mercaptothiazolide)]-N'-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]-bis(2-aminoethyl)amine

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Technology Process of N,N''-bis[3-benzyloxy-1-carbamidomethyl-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl(2-mercaptothiazolide)]-N'-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]-bis(2-aminoethyl)amine

There total 6 articles about N,N''-bis[3-benzyloxy-1-carbamidomethyl-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl(2-mercaptothiazolide)]-N'-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]-bis(2-aminoethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.7%

: 1610625-58-5
N′-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]bis(2-aminoethyl)amine

: 1610625-73-4
3-(benzyloxy)-6-methyl-1-(2-oxo-2-(2-thioxothiazolidin-3-yl)ethyl)-4-(2-thioxothiazolidine-3-carbonyl)pyridin-2(1H)-one

: 1610625-74-5
N,N''-bis[3-benzyloxy-1-carbamidomethyl-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl(2-mercaptothiazolide)]-N'-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]-bis(2-aminoethyl)amine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 47h;

Reference yield:

: 267876-32-4
ethyl 3-hydroxy-6-methyl-2-oxo-1,2-dihydropyridine-4-carboxylate

: 1610625-74-5
N,N''-bis[3-benzyloxy-1-carbamidomethyl-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl(2-mercaptothiazolide)]-N'-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]-bis(2-aminoethyl)amine

Guidance literature:: Multi-step reaction with 5 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / isopropyl alcohol / 4 h / 82 - 83 °C / Inert atmosphere

2: potassium tert-butylate; magnesium 2-methylpropan-2-olate / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

3: sodium hydroxide / ethanol; water / 20 °C

4: dmap; N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 1 h

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 47 h

With dmap; potassium tert-butylate; magnesium 2-methylpropan-2-olate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; isopropyl alcohol;

Reference yield:

: 100-39-0
benzyl bromide

: 1610625-74-5
N,N''-bis[3-benzyloxy-1-carbamidomethyl-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl(2-mercaptothiazolide)]-N'-[2-[2-(2-methoxyethoxy)ethoxy]ethoxy]-bis(2-aminoethyl)amine

Guidance literature:: Multi-step reaction with 5 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / isopropyl alcohol / 4 h / 82 - 83 °C / Inert atmosphere

2: potassium tert-butylate; magnesium 2-methylpropan-2-olate / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

3: sodium hydroxide / ethanol; water / 20 °C

4: dmap; N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 1 h

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 47 h

With dmap; potassium tert-butylate; magnesium 2-methylpropan-2-olate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; isopropyl alcohol;