hexahydro-1H,4H,7H-3a,6a,9a-triaza-9b-phosphaphenalene

Base Information

Chemical Name:hexahydro-1H,4H,7H-3a,6a,9a-triaza-9b-phosphaphenalene
CAS No.:62051-24-5
Molecular Formula:C₉H₁₈N₃P
Molecular Weight:199.236
Hs Code.:

Synonyms:hexahydro-3a,6a,9a-triaza-9b-phospha-phenalene

Suppliers and Price of hexahydro-1H,4H,7H-3a,6a,9a-triaza-9b-phosphaphenalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of hexahydro-1H,4H,7H-3a,6a,9a-triaza-9b-phosphaphenalene

Chemical Property:

Vapor Pressure:0.0118mmHg at 25°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of hexahydro-1H,4H,7H-3a,6a,9a-triaza-9b-phosphaphenalene

There total 4 articles about hexahydro-1H,4H,7H-3a,6a,9a-triaza-9b-phosphaphenalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 294-80-4
1,5,9-triazacyclododecane

: 62051-24-5
hexahydro-3a,6a,9a-triaza-9b-phospha-phenalene

Guidance literature:: With Hexamethylphosphorous triamide; at 120 ℃; for 96h;
DOI:10.1002/ejoc.201201400

Reference yield:

: 5807-14-7,389623-48-7
1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine

: 62051-24-5
hexahydro-3a,6a,9a-triaza-9b-phospha-phenalene

Guidance literature:: Multi-step reaction with 4 steps

1: -20 - 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / -78 - 20 °C

3: sulfuric acid / water / 5 h / Reflux

4: Hexamethylphosphorous triamide / 96 h / 120 °C

With lithium aluminium tetrahydride; sulfuric acid; Hexamethylphosphorous triamide; In tetrahydrofuran; water;
DOI:10.1002/ejoc.201201400

Reference yield:

: C₁₀H₁₈N₃⁽¹⁺⁾*F₆P^(1-)

: 62051-24-5
hexahydro-3a,6a,9a-triaza-9b-phospha-phenalene

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / -78 - 20 °C

2: sulfuric acid / water / 5 h / Reflux

3: Hexamethylphosphorous triamide / 96 h / 120 °C

With lithium aluminium tetrahydride; sulfuric acid; Hexamethylphosphorous triamide; In tetrahydrofuran; water;
DOI:10.1002/ejoc.201201400