5-(benzyloxy)-4-methoxynaphthalen-1-yl 2-iodo-3-methoxy-5-methylbenzoate

Base Information

Chemical Name:5-(benzyloxy)-4-methoxynaphthalen-1-yl 2-iodo-3-methoxy-5-methylbenzoate
CAS No.:133344-06-6
Molecular Formula:C₂₇H₂₃IO₅
Molecular Weight:554.381
Hs Code.:

Synonyms:5-(benzyloxy)-4-methoxynaphthalen-1-yl 2-iodo-3-methoxy-5-methylbenzoate

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Chemical Property of 5-(benzyloxy)-4-methoxynaphthalen-1-yl 2-iodo-3-methoxy-5-methylbenzoate

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Technology Process of 5-(benzyloxy)-4-methoxynaphthalen-1-yl 2-iodo-3-methoxy-5-methylbenzoate

There total 7 articles about 5-(benzyloxy)-4-methoxynaphthalen-1-yl 2-iodo-3-methoxy-5-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 133344-02-2
2-iodo-3-methoxy-5-methylbenzoic acid

: 75445-67-9
5-benzyloxy-4-methoxy-1-naphthalenol

: 133344-06-6
5-(benzyloxy)-4-methoxynaphthalen-1-yl 2-iodo-3-methoxy-5-methylbenzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/S0040-4039(00)97051-5

Reference yield:

: 75445-67-9
5-benzyloxy-4-methoxy-1-naphthalenol

: 140201-79-2
2-iodo-3-methoxy-5-methylbenzoyl chloride

: 133344-06-6
5-(benzyloxy)-4-methoxynaphthalen-1-yl 2-iodo-3-methoxy-5-methylbenzoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2009.11.076

Reference yield:

: 75445-61-3
5-(benzyloxy)-1,4-dihydronaphthalene-1,4-dione

: 133344-06-6
5-(benzyloxy)-4-methoxynaphthalen-1-yl 2-iodo-3-methoxy-5-methylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / Zn, Py / CHCl₃ / Heating; accord. lit.cit.

2: 96 percent / K₂CO₃ / acetone / Heating

3: 60 percent / KOH / methanol

4: 61 percent / DCC, DMAP / CH₂Cl₂

With pyridine; dmap; potassium hydroxide; potassium carbonate; dicyclohexyl-carbodiimide; zinc; In methanol; dichloromethane; chloroform; acetone;
DOI:10.1016/S0040-4039(00)97051-5