C₃₇H₅₄O₂SSi₂

Base Information

Chemical Name:C₃₇H₅₄O₂SSi₂
CAS No.:183610-89-1
Molecular Formula:C₃₇H₅₄O₂SSi₂
Molecular Weight:619.072
Hs Code.:

C<sub>37</sub>H<sub>54</sub>O<sub>2</sub>SSi<sub>2</sub>

Synonyms:C₃₇H₅₄O₂SSi₂

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Chemical Property of C₃₇H₅₄O₂SSi₂

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Technology Process of C₃₇H₅₄O₂SSi₂

There total 12 articles about C₃₇H₅₄O₂SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 882-33-7
diphenyldisulfane

: 183610-88-0
{(1S,2S)-2-[(R)-5-(tert-Butyl-dimethyl-silanyloxy)-1-(tert-butyl-diphenyl-silanyloxy)-pentyl]-cyclopropyl}-methanol

: 183610-89-1
C₃₇H₅₄O₂SSi₂

Guidance literature:: With pyridine; tributylphosphine; Ambient temperature;
DOI:10.1016/0040-4039(96)01692-9

Reference yield:

: 121352-74-7
(2Z)-7-[(tert-butyldimethylsilyl)oxy]hept-2-en-1-ol

: 183610-89-1
C₃₇H₅₄O₂SSi₂

Guidance literature:: Multi-step reaction with 9 steps

1: 1.) powdered 4A molecular sieves, D-(-)-diethyl tartrate, Ti(i-PrO)4; 2.) tert-butyl hyperoxide / CH₂Cl₂ / 1.) 0 deg C; 2.) -20 deg C, 20 h

2: 97 percent / DMAP / CH₂Cl₂ / 2 h / 0 °C

3: 83 percent / 1.) BuLi / tetrahydrofuran / 1.) -78 deg C, 30 min.; 2.) -78 deg C -> room temp. over 5 h, then 1 h

4: 96 percent / dimethylformamide / 4 h / Ambient temperature

5: 92 percent / SmI₂, HMPA / tetrahydrofuran / 0.5 h / Ambient temperature

6: O₃, Me₂S / CH₂Cl₂; methanol / -78 deg C, then -> room temp., 2 h, then room temp., 8 h

7: K₂CO₃ / methanol / 16 h / 50 °C

8: 92 percent / NaBH₄ / methanol / 0.5 h / 0 °C

9: 99 percent / Bu₃P, pyridine / 3 h / 0 °C

With pyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; sodium tetrahydroborate; n-butyllithium; samarium diiodide; dimethylsulfide; diethyl (2S,3S)-tartrate; tributylphosphine; 4 A molecular sieve; potassium carbonate; ozone; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3987/com-97-s(n)58

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 183610-89-1
C₃₇H₅₄O₂SSi₂

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / dimethylformamide / 4 h / Ambient temperature

2: 92 percent / SmI₂, HMPA / tetrahydrofuran / 0.5 h / Ambient temperature

3: O₃, Me₂S / CH₂Cl₂; methanol / -78 deg C, then -> room temp., 2 h, then room temp., 8 h

4: K₂CO₃ / methanol / 16 h / 50 °C

5: 92 percent / NaBH₄ / methanol / 0.5 h / 0 °C

6: 99 percent / Bu₃P, pyridine / 3 h / 0 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; samarium diiodide; dimethylsulfide; tributylphosphine; potassium carbonate; ozone; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3987/com-97-s(n)58