2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-2-N-(4-methoxybenzyl)-L-galactononitrile

Base Information

Chemical Name:2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-2-N-(4-methoxybenzyl)-L-galactononitrile
CAS No.:1602560-23-5
Molecular Formula:C₁₇H₂₂N₂O₄
Molecular Weight:318.373
Hs Code.:

Synonyms:2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-2-N-(4-methoxybenzyl)-L-galactononitrile

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Chemical Property of 2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-2-N-(4-methoxybenzyl)-L-galactononitrile

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Technology Process of 2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-2-N-(4-methoxybenzyl)-L-galactononitrile

There total 3 articles about 2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-2-N-(4-methoxybenzyl)-L-galactononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: potassium cyanide

: 2,3-O-isopropylidene-5-O-p-tolylsulfonyl-L-lyxofuranose

: 2393-23-9
4-methoxy-benzylamine

: 1602560-18-8
2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-2-N-(4-methoxybenzyl)-L-talononitrile

: 1602560-23-5
2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-2-N-(4-methoxybenzyl)-L-galactononitrile

Guidance literature:: With acetic acid; In methanol; at 65 ℃; for 24h; Overall yield = 83 %; Inert atmosphere;
DOI:10.1002/ejoc.201301705

Reference yield:

: potassium cyanide

: 2393-23-9
4-methoxy-benzylamine

: D-lyxose tosylate

: 1602560-18-8
2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-2-N-(4-methoxybenzyl)-L-talononitrile

: 1602560-23-5
2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-2-N-(4-methoxybenzyl)-L-galactononitrile

Guidance literature:: With acetic acid; In methanol; at 65 ℃; for 24h; Overall yield = 88 %; Inert atmosphere;
DOI:10.1002/ejoc.201301705

Reference yield:

: 152139-46-3
2,3-O-Isopropylidene-5-O-(p-tolylsulfonyl)-L-lyxono-1,4-lactone

: 1602560-18-8
2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-2-N-(4-methoxybenzyl)-L-talononitrile

: 1602560-23-5
2,6-dideoxy-2,6-imino-3,4-O-isopropylidene-2-N-(4-methoxybenzyl)-L-galactononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / toluene; dichloromethane / 1.5 h / -78 °C / Inert atmosphere

2: acetic acid / methanol / 24 h / 65 °C / Inert atmosphere

With diisobutylaluminium hydride; acetic acid; In methanol; dichloromethane; toluene;
DOI:10.1002/ejoc.201301705