N-(2,2-di(ethoxycarbonyl)vinyl)-2,3-O-(4-methoxybenzylidene)-β-L-rhamnopyranosylamine

Base Information

Chemical Name:N-(2,2-di(ethoxycarbonyl)vinyl)-2,3-O-(4-methoxybenzylidene)-β-L-rhamnopyranosylamine
CAS No.:678142-31-9
Molecular Formula:C₂₂H₂₉NO₉
Molecular Weight:451.474
Hs Code.:

Synonyms:N-(2,2-di(ethoxycarbonyl)vinyl)-2,3-O-(4-methoxybenzylidene)-β-L-rhamnopyranosylamine

Suppliers and Price of N-(2,2-di(ethoxycarbonyl)vinyl)-2,3-O-(4-methoxybenzylidene)-β-L-rhamnopyranosylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(2,2-di(ethoxycarbonyl)vinyl)-2,3-O-(4-methoxybenzylidene)-β-L-rhamnopyranosylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(2,2-di(ethoxycarbonyl)vinyl)-2,3-O-(4-methoxybenzylidene)-β-L-rhamnopyranosylamine

There total 1 articles about N-(2,2-di(ethoxycarbonyl)vinyl)-2,3-O-(4-methoxybenzylidene)-β-L-rhamnopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 22435-67-2
N-(2,2-diethoxycarbonylvinyl)-β-L-rhamnopyranosylamine

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 678142-31-9
N-(2,2-di(ethoxycarbonyl)vinyl)-2,3-O-(4-methoxybenzylidene)-β-L-rhamnopyranosylamine

Guidance literature:: With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 50 ℃; for 25h; under 20 Torr;
DOI:10.1016/j.tetasy.2004.01.003

Reference yield:

: 678142-31-9
N-(2,2-di(ethoxycarbonyl)vinyl)-2,3-O-(4-methoxybenzylidene)-β-L-rhamnopyranosylamine

: 610314-55-1
1,4-anhydro-N-(2,2-di(ethoxycarbonyl)vinyl)-2,3-O-(4-methoxybenzylidene)-β-L-rhamnopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / pyridine / 24 h / 20 °C

2: 93 percent / sodium methoxide / dimethylformamide / 0.25 h / 40 °C / 20 Torr

With pyridine; sodium methylate; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2004.01.003

Reference yield:

: 678142-31-9
N-(2,2-di(ethoxycarbonyl)vinyl)-2,3-O-(4-methoxybenzylidene)-β-L-rhamnopyranosylamine

: 610314-57-3
1,4-anhydro-2,3-di-O-benzoyl-N-(2,2-di(ethoxycarbonyl)vinyl)-β-L-rhamnopyranosylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / pyridine / 24 h / 20 °C

2: 96 percent / ethanethiol; p-toluenesulfonic acid / CH₂Cl₂ / 4 h / 20 °C

3: 88 percent / pyridine / 24 h / 20 °C

4: 60 percent / sodium methoxide / dimethylformamide / 0.25 h / 40 °C / 20 Torr

With pyridine; sodium methylate; toluene-4-sulfonic acid; ethanethiol; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2004.01.003