2,3-di-O-benzoyl-N-(2,2-di(ethoxycarbonyl)vinyl)-4-O-mesyl-β-L-rhamnopyranosylamine

Base Information

Chemical Name:2,3-di-O-benzoyl-N-(2,2-di(ethoxycarbonyl)vinyl)-4-O-mesyl-β-L-rhamnopyranosylamine
CAS No.:678142-33-1
Molecular Formula:C₂₉H₃₃NO₁₂S
Molecular Weight:619.647
Hs Code.:

Synonyms:2,3-di-O-benzoyl-N-(2,2-di(ethoxycarbonyl)vinyl)-4-O-mesyl-β-L-rhamnopyranosylamine

Suppliers and Price of 2,3-di-O-benzoyl-N-(2,2-di(ethoxycarbonyl)vinyl)-4-O-mesyl-β-L-rhamnopyranosylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,3-di-O-benzoyl-N-(2,2-di(ethoxycarbonyl)vinyl)-4-O-mesyl-β-L-rhamnopyranosylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,3-di-O-benzoyl-N-(2,2-di(ethoxycarbonyl)vinyl)-4-O-mesyl-β-L-rhamnopyranosylamine

There total 4 articles about 2,3-di-O-benzoyl-N-(2,2-di(ethoxycarbonyl)vinyl)-4-O-mesyl-β-L-rhamnopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 98-88-4
benzoyl chloride

: 678142-32-0
N-(2,2-di(ethoxycarbonyl)vinyl)-4-O-mesyl-β-L-rhamnopyranosylamine

: 678142-33-1
2,3-di-O-benzoyl-N-(2,2-di(ethoxycarbonyl)vinyl)-4-O-mesyl-β-L-rhamnopyranosylamine

Guidance literature:: With pyridine; at 20 ℃; for 24h;
DOI:10.1016/j.tetasy.2004.01.003

Reference yield:

: 22435-67-2
N-(2,2-diethoxycarbonylvinyl)-β-L-rhamnopyranosylamine

: 678142-33-1
2,3-di-O-benzoyl-N-(2,2-di(ethoxycarbonyl)vinyl)-4-O-mesyl-β-L-rhamnopyranosylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / PTSA / dimethylformamide / 25 h / 50 °C / 20 Torr

2: 93 percent / pyridine / 24 h / 20 °C

3: 96 percent / ethanethiol; p-toluenesulfonic acid / CH₂Cl₂ / 4 h / 20 °C

4: 88 percent / pyridine / 24 h / 20 °C

With pyridine; toluene-4-sulfonic acid; ethanethiol; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2004.01.003

Reference yield:

: 678142-31-9
N-(2,2-di(ethoxycarbonyl)vinyl)-2,3-O-(4-methoxybenzylidene)-β-L-rhamnopyranosylamine

: 678142-33-1
2,3-di-O-benzoyl-N-(2,2-di(ethoxycarbonyl)vinyl)-4-O-mesyl-β-L-rhamnopyranosylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / pyridine / 24 h / 20 °C

2: 96 percent / ethanethiol; p-toluenesulfonic acid / CH₂Cl₂ / 4 h / 20 °C

3: 88 percent / pyridine / 24 h / 20 °C

With pyridine; toluene-4-sulfonic acid; ethanethiol; In dichloromethane;
DOI:10.1016/j.tetasy.2004.01.003